GCMS analysis results for sample AE08969, May 7, 2002

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’ Data File : C:\MSDCHEM\1\DATA\020424\08969.D vial: 17 Acq On : 25 Apr 2002 1:35 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Methane, bromodichloro- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 3.35 0.21 ug/1 248022 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Methane, bromodichloro- 162 CHBrC12 000075-27-4 72 2 Chloroform 118 CHC13 000067-66-3 64 3 Chloroform 118 CHC13 000067-66-3 64 4 Methane, bromodichloro- 162 CHBrC12 000075-27-4 64 Abundance Scan 47 (3.355 min): 08969.D (-43) (-) m/z 82.95 100.00% 83

5000

48 -HmRn 127 3.20 3.30 3.40 3.50 3.60 3.70 3.80 .................... ..... ................ 191 1 ‘i "■111 ■ ■ ■ i ■ ■ ■ ■ i" 1111'' 'I"'11'1 " r1 +tp " i ■ ■'11"1 ■ i " *H,• i • ’ ’1’4**[*8**1+6**1** 159 m/z 8,5.00 62.48% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #116506: Methane, bromodichloro- 83

5000 s MMi YYMM, AAA Oij 3.20 3.30 3.40 3.50 3.60 3.70 3.80 47 129 m/ z 48.10 14.03% .,, . ........ ... ...... Ih, 55 64 72 11191......... 116 ,, I.)..... 144..... 163 i t t | J > | i | > i > I j i 114 | I 1 t I | > t I < ] I I i > J r t J l II » | l I *anl I J ITi I | "Tgll 1’l’ I l r: | J J I I pm FUTTT j I I miz-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 #116499: Chloroform 83 AwWwpwuut ■ • • i • • “ i" ■11 • ■ ■ • i ■ •111'1111" " I" 3.20 3.30 3.40 3.50 3.60 3.70 3.80 5000 m/z 87.00 13.73% 47

niz-> p Ar 11 ri 1111 35 h -794 1 111'' ■ ■ i ‘ "11 ■''1!1 । ‘' 1111' 1111 ‘11 ‘ ITI 11 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #116498: Chloroform 83 LAA.ANLMAMMA.A, 3.20 3.30 3.40 3.50 3.60 3.70 3.80 m/z 127.00 11.04% 5000 47 35 13..... ..... ..... Ill, ....... 70..... Il............. 118.............................. ... । .-l.. j...) , ■ ’14 I .. ’ l .... j।j । । i i 111 > i rl 11 > n । i 11 > । 111 11 i r, i । 11 i pj 11 ’ ’1444414 “ I “ • H “ “ I' ‘ ‘ * l " 1 r|1» n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 3.20 3.30 3.40 3.50 3.60 370 3.80

08969.D SCAN020424.M Thu May 02 15:00:31 2002 Page 3

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