GCMS analysis results for sample AE10134, May 8 2002

NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\050202\10134 .D Vial: 26 Acq On 3 May 2002 9:42 am Operator: Mclean Sample 4/29 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 1 Methane, bromodichloro- Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

3.32 0.28 ug/L 152474 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methane, bromodichloro- 162 CHBrC12 000075-27-4 90 2 Methane, bromodichloro- 162 CHBrC12 000075-27-4 83 3 Chloroform 118 CHC13 000067-66-3 80 4 Chloroform 118 CHC13 000067-66-3 72 Abundance Scan 40 (3.314 min): 10134.D (-34) (-) m/ z 83.00 100.00% 83

5000 47 > I I I I I I/ .... | I I I 1M i r I I I I i | i r I i |P | I r ........ i r i > |

35 129 3.20 3.30 3.40 3.50 3.60 3.70 ............. I .... Il ........ . ■ I I I I I I I I > I I I I I I I I I I I I I r 11 ■ r '1 ‘ i II 111 1 r ' ■1 r 1111 ITT m/Z 85.00 65.26% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #33236: Methane, bromodichloro- 83

A A____ V A-mmmPTA 5000 I I ( I I I I I I I I I I I

3.20 3.30 3.40 3.50 3.60 3.70 47 m/z 47.10 22.39% 129 13 27 35 63 72 |||, 1 93 116 ||. 164 1'1 r 1111' B’IIU0T1—n’"nTET II, i m/z->______ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 _/ _ Abundance #116497: Methane, bromodichloro- 83 1011 । r । । i r r "i । । । > । । । > । > । * r I T I‘‘I 3.20 3.30 3.40 3.50 3.60 3.70 5000 m/ z 48.10 12.84%

Mo/sPe 47 129

m/z-> TI‘ 10 20 30 40 ,29,27.M.. 50 60 JI 191 111‘01110131/Ttr1‘r‘11"11IT LL 1111 70 80 90 100 110 120 130 140 150 160 170 i'111 r " ' i TIT WAM Abundance #116499: Chloroform '' 11 11 l-l 1 1 1 1 I ' I. I 1 83 3.20 3.30 3.40 3.50 3.60 3.70 m/ z 86.90 12.64%

5000

47 35 1 nIPTmPIPT —4 1 118 TOTITTT. ’’’’b ■ ■ । ■ ■ ■ ■ । ■1 i ■ '1111 1 ' i n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 3.20 3.30 3.40 3.50 3.60 3.70

10134.D 050102.M Mon May 06 12:24:12 2002 Page 4

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