GCMS analysis results for sample AE10134, May 8 2002

NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\050202\10134.D Vial: 26 Acq On 3 May 2002 9:42 am Operator: Mclean Sample 4/29 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 Acetonitrile, dichloro­ Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

3.60 0.51 ug/L 282081 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-1 0 78 2 Allyl mercaptan 74 C3H6S 000870—23-5 16 3 Acetonitrile, dichloro- 109 C2HC12N 0030 3-12-0 16 4 Thiirane, methyl- 74 C3H6S 0-*072-43-1 9 Abundance Scan 89 (3.602 min): 10134.D (-85) (-) m/ z 74.00 100.00% 74

82 5000

47 38 3.20 3.40 3.60 3.80 4.00 ------ .88 Tll I I । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ m/ z 82.00 51.46% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74

5000 82 3.20 3.40 3.60 3.80 4.00 47 m/z 76.00 38.78% 35 . 108 . ........... ,. i'll, , . ............... ..............1 ' 1 1 I 1 1 1 ' i ' 1 1 1 i 1 Til IIIIIII’IIIIII /z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28161: Allyl mercaptan 41 74 I | I I I I । । । । । । w । i i ] i r i i । । r"

3.20 3.40 3.60 3.80 4.00 5000 m/z 84.00 33.58%

27 33 ,| , 47

................ I1' 1 psll] , , 1,53 59 68,,1 ' ■ i 1 ■ 1 1 i ' 1 1 ' i 1 ‘ I I I Di I I I I I I I 1 I ill ■ i ' 1 ■ ■ i wot m/z--> 10 20 30 40। 50 60 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 1 । 1 t ' > । । ' . > । । । । । । । । । । । । । 7|4 3.20 3.40 3.60 3.80 4.00 35 m/z 47.10 22.52%

m/z-> 5000

' 1 i ' 10 ■ ' ■ i 1 1 ■ 1 i 1 1 20 30 -11'1 1 ■ । 40 47

50 60 ■ i ■ 70 80 82

TIl 1 ' । ' 1 1 । 1 1 1 1 । 1 1 ' ' । 90 100 110 w MWMwWWo ■ । ■ 1 ■ ■ । 1 ■ 1 ' । ' 1 1 1 । fl । । । । । 3.20 3.40 3.60 3.80 4.00

10134.D 050102.M Mon May 06 12:24:13 2002 Page 5

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