GCMS analysis results for sample AE10815, May 2002

NYC 9/11 Public Portal Document

‘Data File : C:\MSDCHEM\1\DATA\051402\10815.D Vial : 25 Acq On : 15 May 2002 9:55 am Operator: Mclean Sample : 5/7 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Acetonitrile, dichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 3.63 0.38 ug/L 401875 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Acetonitrile, dichloro- 109 C2HC12N 003018-12 0 91 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 56 3 Thiirane, methyl- 74 C3H6S 001072-43-1 9 4 Allyl mercaptan 74 C3H6S 000870-23-5 9 Abundance Scan 93 (3.626 min): 10815.D (-88) (-) m/ z 74.00 100.00% 74

82 5000 47 35 3.20 3.40 3.60 3.80 4.00 I 58 I o! ■ ■ । 1 TIl I ■ । । । ■ ■ ■ > । ■ ■ ■ ■ । m/z 82.00 54.04% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74

5000 82 A R I ’ ' 1 1 1 1 1 ' 1 1 ' 1 1 1 I ' 1 1 1 I • 1 1 3.20 3 40 3.60 3.80 4.00 47 m/z 84.00 37.08% 35

m/z-> Abundance Of 10 2 2 62 1i]iiiI|inII|riri|IitI|।

20 30 40 50 60 ■ ।

70 1 i 1 ' ' ' i 1 80 #115342: Acetonitrile, dichloro- । | I ■ i ■ ■ ■ • । 90 100 108 > I ' ■ ■ । I 110 MAlt. 7|4 35 i ■ ■ ■ ■ । ■ ■ ■ ' । । । ■ ■ ■ - । ■ 3.20 3.40 3.60 3.80 4.00 5000 82 m/z 76.00 35.80% 47

m/z-> Of 1 ■ i 1 ■ 1 1 । 1 r ■ 1 । 1 10 20 30 l. I, ■ ' ' 60 40 50 ' i ' 1 1 1 i ' 70 80 "dil 1 ■ i 1 1 1 ■ i ' 1 ■ 1 i 1 ■ ' 1 i 90 100 110 Abundance #115343: Thiirane, methyl- nid,T i | | i _1 i I i i | i i i । । i r 41 7|4 3.20 3.40 3.60 3.80 4.00 m/z 47.00 25.00%

5000

0 27 33 , 47 + 111,53 5968 1 I ■ । । । ■ ■ ■ ■ । ■ ■ ■ ■ । • ■ ■ > । w/lw WWMwyarta i 1 1 1 1 i ' 1 ' 1 I1 I I I I I I I I 1 I [ III I I I kl I I I I

/z-> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.40 3.60 3.80 4.00

10815.D 050102.M Thu May 16 14:17:24 2002 Page 5

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