GCMS analysis results for sample AE09335, May 2002

NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\050202\9335.D Vial : 13 Acq On 2 May 2002 9:27 pm Operator: Mclean Sample 4/29 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Acetonitrile, dichloro- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

3.63 0.30 ug/L 289979 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 3 3,3-Dichloropropyne 108 C3H2C12 1000222-23-9 4 Allyl mercaptan 74 C3H6S 000870-23-5 Abundance Scan 94 (3.632 min): 9335. D (-88) (-) m/z 74.00 100.00% 7|4

82 5000

40 47 । । > 3.20 .. 4..... 3.40 3.60 3.80 4.00 11 1.............. 1,l1 ' ' Il ' ' ' 1 i • 1 ■ ■ i 1 I m-1 88 11111191’ m/ z 82.00 56.60% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 7|4

5000 82 ...N.......... 3.20 3.40 3.60 3.80 4.00 47 m/z 84.00 38.57% 35 - /z—> i I ।

10 2 20 I

30 I

40 I

50 I | 1 I I i [ r i i I | I I I

60 i । । i m-1 r

80 62 1 1 । 1 70 । | I 1 । 1 1 1 ' p ' 1 1 I 1 1 1 1 i 90 100 108 110 Abundance #115342: Acetonitrile, dichloro- 74 35 3.20 3.40 3.60 3.80 4.00 5000 82 m/z 76.00 34.33% 47

1 ' i 1 1 ■ 1 i ■ ■ 1 ■ i 1 '"1 1 —P— ■ i ■ ' 1 ■ i 1 TIl 1 1 । 1 1 1 1 । ■ ■ ■ ■ । 1 ■ 1 ■ । m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28312: 3,3-Dichloropropyne 74 3.20 3.40 3.60 3.80 4.00 m/z 47.05 24.45%

5000 38 47 Mwa/vt) m/z-> 1 ' i 1 1 1 ' i ' 10 20 2. .mu,, 30 40 Ii 53 60 1 1 i ■ ■ 1 ■ 1 1 1 ' ■ 1 1 50 60 70 j 80 82 90 108 1 i 1 1 ■ ' i ■ ■ ■ 1 i 1 r 1 1 i ■ ' ■ 1 i 100 110 । ■ ■ ■ 3.20 ■ । ■ ■ ■ ■ । 3.40 3.60 । । ■ 1 । ■ । । । 3.80 4.00

9335.D 050102.M Mon May 06 13:59:43 2002 Page 6

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