GCMS analysis results for sample AE08970, May 7, 2002

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Laboratory report documenting GCMS analysis of sample AE08970 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000049658–000049670

Folder label: “GCMS X 4/16/02 A 4/24/02”

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NYC 9/11 Public Portal Document

'Data File : C:\MSDCHEM\l\DATA\020424\08970.D Vial: 18 Acq On : 25 Apr 2002 2:34 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Methane, bromodichloro- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

3.35 0.22 ug/1 259928 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methane, bromodichloro- 162 CHBrC12 000075-27-4 78 2 Methane, oxybis [dichloro- 182 C2H2C140 020524-86-1 64 3 Methane, bromodichloro- 162 CHBrC12 000075-27-4 64 4 Methane, bromodichioro- 162 CHBrC12 000075-27-4 64 Abundance Scan 46 (3.349 min): 08970.D (-43) (-) m/z 82.95 100.00% 83

5000

48 M Al । NIJIYMMM 14TM *

miz-> m 36 58 ■ ■I, , .92... r. . .. 1 1I1 ‘ ' 1 I 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 129 ' I “ “I “ “ I ■ “ > 1M . I| M M] M . .| . 3.20 3.30 3.40 3.50 3.60 3.70 3.80 m/z 85.00 77.06% Abundance #116496: Methane, bromodichloro- 83

5000 MMMA YMM AWA M Mit 3.20 3.30 3.40 3.50 3.60 3.70 3.80 47 m/z48.05 20.92% 35 129

miz-> 13 “ • i“ i • • +,58..70 -4 I9,1, 116 ||, 111111111 nil 1111 I’i ’rr । j hi . 111111 11 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 164■ । ■ i

Abundance #33237: Methane, oxybis[dichloro- 83 AAA—Wh/lynW/ 3.20 3.30 3.40 3.50 3.60 3.70 3.80 5000 m/z 47.05 20.72% 47 28

m/z-> 7 —7 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 II | »»»• p •• u ««••]*“» p ••• l • •

Abundance #116497: Methane, bromodichloro- '■i“ “i"" i'“‘i"1''i111‘i "“i11 83 3.20 3.30 3.40 3.50 3.60 3.70 3.80 m/z 128.90 14.83% 5000

28 47 129 2.37,.., n 191 II, T| » ... 11 I . ‘1’’** | l‘ ‘ ‘ ‘«I•‘ ‘ ‘ «’143 niiHipm 11» » * J » 1 TTp-m-pTT ’I t । IpIIJ|JMI|JJ m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 3.20 3.30 3.40 3.50 3.60 3.70 3.80

08970.D SCAN020424.M Thu May 02 15:01:16 2002 Page 3

NYC-WTC_000049664

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GCMS analysis results for sample AE08964, May 7, 2002 · Box DEP Box 27

NYC-WTC_000049622

Laboratory report documenting GCMS analysis of sample AE08964 conducted on May 7, 2002, by analyst DLV.

1 shared topics · Same agency, volume and box · similarity 0.997