GCMS analysis results for sample AE08963, May 7, 2002

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Laboratory report documenting GCMS analysis of sample AE08963 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000049609–000049621

Folder label: “GCMS X 4/16/02 A 4/24/02”

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NYC 9/11 Public Portal Document

•Data File : C:\MSDCHEM\1\DATA\020424\08963.D Vial: 14 Acq On : 24 Apr 2002 10:39 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Methane, bromodichloro- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

3.35 0.22 ug/1 280048 1,4-Dichlorobenzene-d4 11.38 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Methane, bromodichloro- 162 CHBrC12 000075-27-4 83 2 Methane, bromodichloro- 162 CHBrC12 000075-27-4 83 3 Methane, bromodichioro- 162 CHBrC12 000075-27-4 78 4 Methane, bromodichioro- 162 CHBrC12 000075-27-4 74 Abundance Scan 46 (3.349 min): 08963.D (-41) (-) m/z 82.95 100.00% 83

5000 47 *ANpYMP4fAf 127 3.20 3.30 3.40 3.50 3.60 3.70 3.80 — 11. 316 1' i ■ ■ I ‘• I “ ‘' I • • “ I ‘ ‘ • I ‘ “ I “ ‘* I TT ।.... i.... ।...11. m/z 84.95 64.75% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #116496: Methane, bromodichloro- 83

abspojpwodlkepopapnopptppotopo 5000- 3.20 3.30 3.40 3.50 3.60 3.70 3.80 47 m/z 47.00 23.42% 129 13 TfTT —*A3.4l4+114.1, 6 ut W ’1’2111111110TOIB—33’1""UETT’ICOIG-T"ITTIAITT miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #116506: Methane, bromodichloro- 83 12191515—0—2—19—0098003382 3.20 3.30 3.40 3.50 3.60 3.70 3.80 5000 m/z 40.10 21.92%

47 129 13 28 TPH ,64.1141144163 ....................................... fpr. ।». • 11 174 j 111 i j |Ti j i j» i u । ।»i ij 1111 j»11 j 111 u |t i TIT+ 111 !■ n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #33236: Methane, bromodichloro- ~1110000110107001090009088281 83 3.20 3.30 3.40 3.50 3.60 3.70 3.80 m/z 48.05 15.45% 5000

47 • 129 13 28, 163 1.114 II,...... 164......................... mpy i111 ‘1444477 . I ‘ ‘1 I‘1‘.| “ " I > | I | 1 U I || I I I 1 | I I I I | I H . | I • • ............ । ।n > ■ 11 p 1111 ■ । n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 3.20 3.30 3.40 3.50 3.60 3.70 3.80

08963.D SCAN020424.M Thu May 02 14:52:33 2002 Page 3

NYC-WTC_000049615

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GCMS analysis results for sample AE08960, May 7, 2002 · Box DEP Box 27

NYC-WTC_000049571

Laboratory report documenting GCMS analysis of sample AE08960 conducted on May 7, 2002, by analyst DLV.

1 shared topics · Same agency, volume and box · similarity 0.998