GCMS analysis results for sample AE08963, May 7, 2002

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Data File : C:\MSDCHEM\1\DATA\020424\08963.D Vial: 14 Acq On : 24 Apr 2002 10:39 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Acetonitrile, dichloro­ Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 3.65 0.25 ug/1 312553 1,4 -Dichiorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 78 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 72 3 Thiirane, methyl- 74 C3H6S 001072-43-1 5 4 Allyl mercaptan 74 C3H6S 000870-23-5 5 Abundance Scan 97 (3.649 min): 08963.D (-92) (-) m/z 74.05 100.00% 74

82 5000 47 Ppp 40 3.40 3.60 3.80 4.00 + ............... ] 1... 411187,... ■ i ■ ■ ' ■ i ■ ' ■ ' i m/z 82.00 57.83% niz->10 20 30 40 50 60 70 90 100 110 80 Abundance #115342: Acetonitrile, dichloro- 74 35

5000 82 AA t f 4++4 PAAP—— 3.40 3.60 3.80 4.00 47 m/z 76.00 30.93%

• • ■ i ■ ■ 1 1 1 1 1 1 ' 1 1 1 1 — ' i ' ’ • • l • ■n-1 141*4111****1* iz->_______10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74 .................... M.................... ‘ *I*!*I* ■ ■ । । । i i ■ । 1 1 1 3.40 3.60 3.80 4.00 5000 82 m/z 47.10 27.29% 47

niz-> Abundance 12 1 ■ i 11 1 ■ i ■ 10 20> 35 230 440— —2— TF4 80 , 108 '1111 r 1111 Ittm • ■ 1 50 60 70 #115343: Thiirane, methyl- 90 100 110 wWpusdt. ‘•I*‘I**‘*I-‘I** 41 74 3.40 3.60 3.80 4.00 m/z 84.00 26.03% 5000 Jrmno/ WWMAu 47

m/z—> ........ 10 20 77,33. 30 |l|l|.l|l.,S, 40 50 60 70 —mmmm 80 90 100 110 1 ■ i ■ ■ ■ ■ i 1 1 1 11 1 1 1 ■ i 1 1 3.40 3.60 3.80 4.00

08963.D SCAN020424.M Thu May 02 14:52:35 2002 Page 4

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