GCMS analysis results for sample AE08959, May 7, 2002

NYC 9/11 Public Portal Document

•Data File : C:\MSDCHEM\1\DATA\020424\08959.D Vial: 10 Acq On : 24 Apr 2002 6:43 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 3.65 0.22 ug/1 277584 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 90 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 39 3 Allyl mercaptan 74 C3H6S 000870-23-5 25 4 Thiirane, methyl- 74 C3H6S 001072-43-1 9 Abundance Scan 97 (3.649 min): 08959.D (-93) (-) m/z 74.00 100.00% 74

5000

35 1111404,58.. 47 1)4

220 m/z82.00 3.40 A 3.60 3.80 4.00 71.29% • • i • 11l miz-> 20 60 80 100 120 140 160 180 200 220 Abundance #28338: Acetonitrile, dichloro- 74

50001 ■ ■ fi II -MMPPP IM 3.40 3.60 3.80 4.00 47 m/z76.00 35.01% 35 _’ ‘121 ‘ I 25 ,1,Il _ ||. 62 11 1 1 1 ’ 1 • * । * * 108 It 1 1 1 I ■ r' 1 i • • • ■ i ■ • ■ ■ i ■ ■ ■ 1 i ‘ • i ■ • • ■ i • ' niz-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #115342: Acetonitrile, dichloro- 74 35 __1 ■ ■ ■__ | A■ i • • 1 ’ i 1 ■ ■ i ■ ■ ' ‘ i ■ f 3.40 3.60 3.80 4.00 m/z 84.00 29.14%

w"awwuu. 5000 47 IM

n llorpe ■ miz-> Abundance ■ ■ i ■ ■ 20 40 60 80 100 120 140 160 180 200 220’ #28161: Allyl mercaptan ■ 1 i ' ■ ■ 1 i • ■ ■ ■ I' 1 1 1 1 1 1 1 41 7* 3.40 3.60 3.80 4.00 m/z 47.10 28.28%

iz—> 5000

27 —l h0 t 59 20 1 rl , 11.1llr,1 .......... I .... 1 ... .... ...... 40I 60 80 100 120 140 160 180 200 220 vwytWAany/ w ■ ■ i ■ • 1 1 i 1 1 1 1 i ‘ 1 1 ' i 1 1 3.40 3.60 3.80 4.00

08959. D SCAN020424.M Thu May 02 14:41:11 2002 Page 3

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