GCMS analysis results for sample AE10702, May 20 2002

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- Data File : C:\MSDCHEM\l\DATA\020513\10702.D Vial: 13 Acq On : 14 May 2002 12:24 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 3.65 0.47 ug/1 41979 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 94 2 Ace nitrile, dichloro- 109 C2HC12N 003018-12-0 64 3 All 1 mercaptan 74 C3H6S 000870-23-5 25 4 Chi) ral Hydrate 164 C2H3C13O2 000302-17-0 25 Abundance Scan 97 (3.649 min): 10702.D (-93) (-) m/z 74.00 100.00% 74

5000 47 ■ 1 । ■ 112 X— . । । r • > 3.40 3.60 3.80 4.00 | 108 528 i ■ ' I 1 ' m/ z 82.00 50.58% -n/z~> 0 50 100 150 200 250 300 350 400 450 500 Abundance #28338: Acetonitrile, dichloro- 74

5000 • t , 44 , A ।— ...... 47 3.40 3.60 3.80 4.00 m/ z 76.00 35.74% 12l ■ . ,108 i ■ ■ ■ n/z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #115342: Acetonitrile, dichloro- 74 35 ...................... / W,A 3.40 3.60 3.80 4.00 5000 m/z 84.00 32.04%

zwMhLdpkuonyy. ' I ' ' ' 1 1 ' ' 1 ' 1 1 ' 1 ' 1 1 1 ' 1 I ' ' ' 1 1 1 1 1 1 I 1 1 1 1 I 1 1 1 1 1 1 ' 1 1 1 1 1 n/z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #28161: Allyl mercaptan ‘ ' i ■ 1 ■ 1 1 1 1 1 411 74 3.40 3.60 3.80 4.00 m/z 47.00 31.03% 5000

Ajow/ywow WMoWho __ iL J l .1 ill _________ __ ______________ i 1 11' ' i ' 1 ' ' i ' ' ' ' i 1 ' 1 ' i ‘ ' i ' ......... m/z—> 0 50 100 150 200 250 300 350 400 450 500 3.40 3.60 3.80 4.00

10702.D SCAN020507.M Wed May 15 08:44:05 2002 Page 3

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