GCMS analysis results for sample AE10702, May 20 2002

NYC 9/11 Public Portal Document

■ Data File : C:\MSDCHEM\l\DATA\020513\10702.D Vial: 13 Acq On : 14 May 2002 12:24 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 2-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

5.33 0.49 ug/1 44183 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H140 000626-93-7 50 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 50 3 5-[2/(Dimethoxyphosphoryl)acetox... 280 C10H17O7P 1000187-38-4 40 4 2-Hexanol 102 C6H140 000626-93-7 39 Abundance Scan 383 (5.330 min): 10702.D (-379) (-) m/z 45.10 100.00% 45

5000

*rtIttMi ITM .-I r r 69 5.00 5.20 5.40 5.60 55 1 87 107 204 > I I I I I I I I I I 1 I I I I ■ I I ) I < I I I I I I I I 1 > I I I I I > I I I I ■ I I I I ' I ■ I I I I ■ P"1 r 1"r1" i11 " r111 r 111 r "'r1 ’111r 1 m/z 41.10 23.23% n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #110734: 2-Hexanol 45

AobuauddadsatA 5000 5.00 5.20 5.40 5.60 m/z 43.05 21.59% .5 H I 27 69 55 87 n/z-> Abundance T^TT 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210

45 T11" "102 r ■" r'" i"'' r "' rr" r ■" r " ■ r " ■ r ‘ "i" " I" "I''

#110825: 2-Pentanol, 4-methyl- MPpMy/WW lwsa ■ ' i ■ 1 1 ■ i ■ 1 ' 1 i 1 1 1 1 i ' ' 1 ' i 5.00 5.20 5.40 5.60 5000 m/z 69.20 12.78%

69 ,"1 527 57 I|.. 87,,101......................... ■ r"1 r ' 1’7 111111 h ।, jY.... । 'T' " 1 I ' 1 ' ‘ 1 1 ' " I ' 1 rl ’ 1 1 ' 1 1 1 1 ' I ' 1 H I ' ' ' j I ' 1 ' ' I ' ' 1 ' 1 1 1 ' 1 | ' 1 ' ' | 1 ' 1 ' | ' ' 1 ' | .......... / m/z-> Abundance 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 #11879: 5-[2-(Dimethoxyphosphoryl)acetoxy]hex-2-enoic acid 45 86 ■' ।''111 ■ ■171 ■' 1A 1 1 । 1 1 r ■ । 5.00 5.20 5.40 5.60 m/z 39.15 6.08% 68 5000

/z-> ..... Mr HH I 1.137 27

TiT’a 11 Trr i'| II i'i . .... . ■ 11 r|'i..... i 57 169> ................. ... ...... 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 96 109 i > 11 ■ i ■ ■ 11 ■ ■ r| 11 < r-p ■ 127 150 MAAqeildebi hulAAnd 5.00 5.20 5.40 5.60

10702.D SCAN020507.M Wed May 15 08:44:06 2002 Page 4

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