GCMS analysis results for sample AE10019, May 2002

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Data File C:\MSDCHEM\1\DATA\020507\10019.D Vial: 18 Acq On 8 May 2002 4:53 am Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 3-Penten-2-ol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 5.80 1.63 ug/1 125110 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 -Penten-2 -ol 86 C5H10O 001569-50-2 59 2 1-Hexene, 4,5-dimethyl- 112 C8H16 016106-59-5 42 3 3 -Penten-2 - ol 86 C5H10O 001569-50-2 42 4 1-He ene, 4-methyl- 112 C8H16 013151-05-8 38 Abundance Scan 463 (5.800 min): 10019.D (-458) (-) m/z 41.10 100.00% 41 71 5000

53 58 84 5.40 5.60 5.80 6.00 6.20 Tr r 1" i" " i'1" I " " i 34 +++654 - m/Z 43.05 94.04% /z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #24376: 3-Penten-2-ol 43 71

5000 1 1 । 1 1 27 53 5.40 5.60 5.80 6.00 6.20 m/z 71.10 61.77% 15 86 +1l,32,,1 44 58 65 | 111 111111111111il111 I "i" " i" " 111" r"11"111" "i1 Tl/z-> i5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #6302:1 -Hexene, 4,5-dimethyl- 43 71 1* t Arim*i 114 TPt fr 5.40 5.60 5.80 6.00 6.20 5000 55 m/z 69.10 47.47%

27

m/z—> 5 T 15 i" " i1 >" i ■ ■ "Jlli..... I|ll +I++ 651 11,1111111 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 , 010000*010000 77 84 97—01—3 — Abundance #114530: 3-Penten-2-ol 71 5.40 5.60 5.80 6.00 6.20 43 m/ Z 39.05 43.34% 5000 53 27 38 i । 58 65 86

n/z-> IIBII 433,21 l 48 I । 4 _81 4-rm ||| ll 11 I11 | IIIi1 I 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 1 ,TI | 1 । । | | i | | 1 | r

5.40 5.60 5.80 6.00 6.20

10019.D SCAN020507 ,M Tue May 14 08:39:36 2002 Page 4

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