GCMS analysis results for sample AE10020, May 2002

NYC 9/11 Public Portal Document

‘Data File C:\MSDCHEM\1\DATA\020507\10020.D Vial: 19 Acq On 8 May 2002 5:52 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Pentane, 1-(1-methylethoxy)- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 5.80 3.16 ug/1 285055 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentane, 1-(1-methylethoxy)- 130 C8H18O 005756-37-6 38 2 1-Heptene, 4-methyl- 112 C8H16 013151-05-8 38 3 1-Tr.ifluoroacetoxy-2-methylpentane 198 C8H13F302 1000215-95-6 37 4 1-Hexene, 4-ethyl-______________ 112 C8H16 016746-85-3 35 Abundance Scan 463 (5.800 min): 10020.D (-456) (-) m/z 41.10 100.00% 41

69 5000

—Tuu——m——TPTr 5.40 5.60 5.80 6.00 6.20 .486 105.. ' I I I I I I I I I I I I I I I 1 ] 1 I I 1 I I I I 229 306 1I‘III77T-T‘11"7‘1111111111711111111100011711TT 346 1‘k1 m/z 43.10 80.65% /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #109923: Pentane, 1-(1-methylethoxy)- 43

71 5000 5.40 5.60 5.80 6.00 6.20 115 m/z 69.10 54.76% 2, 87. 1,,, ,■..................... '' I " '' I H1r ' i'''11" " i' " 11" " I ■' " i " 111" " I " " I " " I " 111 " " I " " I " " I " " 111 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #6181:1-Heptene, 4-methyl- 43 70 - Mni ' 5.40 5.60 5.80 6.00 6.20 5000 m/ Z 39.10 50.00%

n/z-> Abundance 27 —LH, T TTTuumuDTPTmuuBTTTT 20 112 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340

43 #6107:1-Trifluoroacetoxy-2-methylpentane

69 1 AITR1811 . —TT11 1 5.40 5.60 5.80 6.00 6.20 m/z 71.10 L 46.89% 5000

85

/z-> n20..401460, 80 100 120 140 160 180 200 220 240 260 280 300 320 340 —11* 5.40 5.60 5.80 6.00 6.20

10020.D SCAN020507.M Tue May 14 08:44:23 2002 Page 4

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