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GCMS analysis results for sample AE10021, May 2002

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Laboratory report documenting GCMS analysis of sample AE10021 conducted on May 14, 2002, identifying unknown compounds.

NYC-WTC_000044144–000044155

Folder label: “GCMS X 4/26/02 A 5/8/02

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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\020507\10021.D vial : 20 Acq On 8 May 2002 6:51 am Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 1-Heptene, 4-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

5.80 1.98 ug/1 182321 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Hept ene, 4-methyl- 112 C8H16 013151-05-8 64 2 1-He: ne, 4,5-dimethyl- 112 C8H16 016106-59-5 50 3 Fura , tetrahydro-2-(methoxymeth... 116 C6H1202 019354-27-9 50 4 1-Butanol, 2,3-dimethyl- 102 C6H140 019550-30-2 47 Abundance Scan 463 (5.800 min): 10021 .D (-457) (-) m/z 41.10 100.00% 41

69 5000

--------- 86 - 5.40 5.60 5.80 6.00 6.20 mH 1 ' I 11 " | ' 1 1 1 " 1 I ’ " ' 1 1 " ' I ' " ' I " " I 1 1 1 1 1 1 " 1 I " 1 1 I 1 " 1 I " " I " " I " " I 371 j |j ""I 335 m/z 43.10 75.07% /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #6181: 1-Heptene, 4-methyl- 43 70

5000 5.40 5.60 5.80 P 6.00 6.20 m/ Z 69.10 60.84% 15 | j 112 Tdvvvp > ■ I I I ■ I < I I I I ■ > I I I I I I < I I I I I I I I I I I I I I I I I TTTPPTT i" " i ‘ ' r ■111 /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #6302: 1 -Hexene, 4,5-dimethyl- 43 71 a Yr 1T 1 -/>- । 5.40 5.60 5.80 6.00 6.20 5000 m/z 71.10 53.21%

fl | 1 t I ) > | ! I I I | I I ■ I | I I I I | I I 1 I'p I I I | I I I I | I I I I | 15.4 4 r " ' i " " r ‘ " i" " r " ' i" '' i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #114520: Furan, tetrahydro-2-(methoxymethyl)- TTTI—v“*-T “MP 71 5.40 5.60 5.80 6.00 6.20 m/ z 39.10 42.98% 43 5000

97 116 ■ ■ । ‘ ■ I 1 ) '' i" r' i ■ " 1 r " ' r 1 ’ ■ i " ‘1 r 1" 11" 111 " 11 " " I " 111" " r 11' 11 " ' I'1 " I ■r y. 1-, •, । r ,-i t । । i''।-1--i । । । । n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 5.40 5.60 5.80 6.00 6.20

10021.D SCAN020507.M Tue May 14 08:44:51 2002 Page 4

NYC-WTC_000044151

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NYC-WTC_000044151Source: NYC Law Department, mirrored locally

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