GCMS scan report for Method 508, April 2002

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Data File : C:\MSDCHEM\l\DATA\020419\08430.D Vial: 17 Acq On : 19 Apr 2002 11:53 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 1,6-Heptadien-4-ol Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 5.80 0.70 ug/1 979555 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,6-Heptadien-4-ol 112 C7H120 002883-45-6 64 2 Furan, tetrahydro-2-(methoxymeth. .. 116 C6H12O2 019354-27-9 56 3 3-Penten-2-ol 86 C5H10O 001569-50-2 45 4 1,6-Heptadien-4-ol 112 C7H12O 002883-45-6 40 Abundance Scan 463 (5.799 min): 08430.D (-456) (-) m/z 41.15 100.00% 41 71

5000

53 5.40 5.60 5.80 6.00 6.20

m/z-> 01 20 36 011011/0 30 40 1471 50 61.1] 60 70 ! 84 , ____________ 1III1+—))1mTTTT I 80 90 100 110 120 m/z 71.10 88.94% Abundance #24354:1,6-Heptadien-4-ol 43 71

5000 5.40 5.60 5.80 6.00 6.20 27 m/z 43.20 88.39%

iz-> 0- —+37l +74+654 117,84...9.............. 20 30 40 50 60 70। 80 90 100 110 120 Abundance #114520: Furan, tetrahydro-2-(methoxymethyl)- 71 TIYPIMP 43 5.40 5.60 5.80 6.00 6.20 5000 m/z 69.10 53.08%

0- I , 51 ,58 65 I,.......... 85 97................ 116

4 ' ' i ' 1 ‘ 1 1 ' 1 1 ' | 1 । 1 ' i i'i'i'l m/z-> Z) 30 40 50 60 70 80 90 100 110 120 Abundance #114530:3-Penten-2-ol ‘1 14 f’ । 71 5.40 5.60 .6.00 6.20 5.80 43 m/z 39.20 49.89% 5000 A 53 27 86 0 21 ' ' I ' 141,1,1/13711148,4 +59.47 1I Pr । । । । । ■ । । । i । AAA A ■ i 1 ■ ■ ■ i 1 ■ ■ ' i 11 1 kaa 11 PIt 1 n/z-> 20 30 401 50 60 701 80 90 100 110 120 5.40 5.60 5.80 6.00 6.20

08430.D SCAN020418.M Mon Apr 29 08:29:47 2002 Page 17

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