GCMS sample analysis results for AE10698, May 20 2002

NYC 9/11 Public Portal Document

'Data File : C:\MSDCHEM\1\DATA\020513\10698.D Vial: 9 Acq On : 13 May 2002 8:26 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 1 Acetonitrile, dichloro- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 3.65 0.43 ug/1 30075 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 56 2 2 etonitrile. dichloro- 109 C2HC12N 003018-12-0 50 3 2 llyl mercaptan 74 C3H6S 000870-23-5 9 4 2 cetaldehyde, trichloro- 146 C2HC130 000075-87-6 9 Abundi ice Scan 97 (3.649 min): 10698.D (-92) (-) m/z 74.00 100.00% 74

5000 47 —...................... A , I-, । , 3.40 3.60 3.80 4.00

m/z-> .44.,.. 20 40 60 108 66 146 TIt T1}umuBCWWOIWOT 80 248 100 120 140 160 180 200 220 240 m/z 84.00 65.93%

Abundance 74 #28338: Acetonitrile, dichloro-

„MlMlan/opotoyi 5000 r' I 1 1 1 1 1 1 1 3.40 3.60 3.80 4.00 47 m/ z 81.90 54.22% 35 ■ 12 24 |,|| | | 62 TIt86 ' 1 i 108 I I I I I I_ I r I ■ I > I I I I I ' 1 ■ ■ i 1 ' ■ 1 i 1 1 1 ■ i 1 ■ 1 1 1 1 1 1 1 1 1 1 ' 1 1 mn 1 i 1 ' n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #115342: Acetonitrile, dichloro-

35 7|4 A A L A-AA-A-A-A— ——YMAH-A,—————r 3.40 3.60 3.80 4.00 5000 m/z 47.05 34.14%

47

n/z-> ‘II" 20 4 40 1 i ■ ■ 60 80 86 1 1 । ‘ 1 1 ■ ।1 1 1 11 ■' ■ ■ । 1 1 1 1 । • ■ ■ ■ । 1 ■ 1 1 । 1 11 1 । 1 ' 100 120 140 160 180 200 220 240 y»"MWMA/Mybswhouspy Abundance #28161: Allyl mercaptan 1 1 1 1 1 1 I 1 1 1 4f1 74 3.40 3.60 3.80 4.00 m/ z 76.00 31.92% 5000

27 I 59 ji.lIIi............................................ .111Il, , ,.i "I 1 1 1 1 । 1 i 1 ■ 1 1 i 1 1 1 1 i 1 1 ' 1 i 1 11 1 i ' 1 1 1 i 1 1 1 1 I 1 1 1 1 I 1 1 I 1 1 n/z--> 20 40> 60 80 100 120 140 160 180 200 220 240 3.40 3.60 3.80 4.00

10698.D SCAN020507 .M Wed May 15 08:33:44 2002 Page 3

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