GCMS sample analysis results for AE10698, May 20 2002

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' Data File : C:\MSDCHEM\1\DATA\020513\10698.D Vial: 9 Acq On : 13 May 2002 8:26 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 6.12 0.86 ug/1 60523 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 56 2 Ethanol, 1,2,2-trichloro- 148 C2H3C130 000115-20-8 12 3 Ethanol, 2,2,2-trichloro- 148 C2H3C130 000115-20-8 9 4 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 9 Abundance 7 Scan 518 (6.123 min): 10698.D (-512) (-) m/z 43.10 100.00% 43

5000 ...... N TT-n-r 1 1 I 1 1 ' 1 I ' ' 1 82 97 . 117 127 5.80 6.00 6.20 6.40 ' 1 ' | , I 'mm| ' lk 35’i | । ’itlp ' 1 | ■ I ■ ' | 1 l’ 63 ||,|,|| I'l'1mpmegr .061711 1 1 1 I ।11,1 '1'1 'l 1 1‘ ।1 ''1'1'1 I i I I I i i |‘|' | i ' ' I i I i i I i i I i I i i i |-r ' 1 1 ' ’ i i i ’111 I 'I I 'I I I I J m/z 127.00 9.20% m/z->______ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #3877: 2-Propanone, 1,1,1 -trichloro- 43

5000 .............. MA ■ ' ' I ■ ■ ' ■ I ■ 1 1 ■ I ' ■ I ■ I 1 1 I I I 5.80 6.00 6.20 6.40 m/z 124.90 9.15% 15 1 ■ - । । 27 36 , ,50 63 76 83 97 110117 125 । ■ rH+ 1 1 1 I ’ ’’ 1’ ’ ' i ■ '1 ■ i1,1 ■ i '1 ' ''I 1 1 1 1 ।' 1 ' ' । 11 i-| iii ■| 1 1 1 1 i 1 1 1 1 i ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #108334: Ethanol, 2,2,2-trichloro- 31 ■ 1 ■ ।' 1 1 ' । 1 ■ 1 1 । 1 1 1 1 i 1 1 1 1 । 5.80 6.00 6.20 6.40 5000 m/z 81.90 8.30%

49 77 ।1 । ■ 11 1 । 14 — 42 . 61 |, 84 148 95 113,121 i ।' I । । li ।11 | । । । । | ‘ । r । । । । । I I' [ I'i'i > । ■ *111 ■1'11'' । ''i ■ 11111111111111111' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #108333: Ethanol, 2,2,2-trichloro- 1 1 1 i ' 1 IAA 31 5.80 6.00 6.20 6.40 m/z 83.00 6.44%

5000

49 77 18 , . 42 „I, 61 70L 84 95 113,21128135 148 a MW A Pw AA Aa I " 11 1 " 11 i j i “Ft r।■ t'i i r| । ।' i । |'i । i T I 1 1 ' ' 1 1 1,1 I ' 1 1 ' I । । । । |'i । i r-j-i i i । । i-i i i । - i i p i i

m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 5.80 6.00 6.20 6.40

10698.D SCAN020507 .M Wed May 15 08:33:46 2002 Page 4

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