GCMS sample analysis results for AE10699, May 20 2002

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Laboratory report detailing GC/MS analysis of sample AE10699 including surrogate recovery data in May 2002.

NYC-WTC_000045721–000045734

Folder label: “GCMS X 5/3/02 A 5/13/02”

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NYC 9/11 Public Portal Document

‘ Data File : C:\MSDCHEM\1\DATA\020513\10699.D Vial: 10 Acq On : 13 May 2002 9:25 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C: \MSDCHEM\1\METHODS\SCAN020507 . M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 6.13 0.51 ug/1 45383 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

S 1 2 -Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 42 2 Ethanamine, 2-(ethylthio)-, hydr... 141 C4H12C1NS 054303-30-9 9 3 2-Propen-I-ol, 2-chloro-, acetate 134 C5H7C1O2 000692-72-8 9 4 Ethene, chloro- 62 C2H3C1 000075-01-4 9 Abundance / Scan 519 (6.129 min): 10699.D (-514) (-) m/z 43.10 100.00% 4(3

5000

■ ■ i . ■ . . i . . . ■ i . ■ ■ . । . . . . । 5.80 6.00 6.20 6.40 111 1 '' i' ‘1 111111,1 A 35 51 61 73 125 1171111))32Uk)37 Phn idue peui r| |l|', . | . 1111/*/’’ 83 97 m/z 125.00 8.40% /z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #3877: 2-Propanone, 1,1,1-trichloro- 43

5000 ................ tin................... .. 5.80 6.00 6.20 6.40 m/z 49.05 6.13% 15. 27 36 /z-> Abundance ,50 63 76 83 97 110117 125 i i । r I i i । i irr| । i’l’i ’I I ' 1' | 1 . 1 ' r' . ■1 1 | ' 1 1 I | 11111 1 | • r i >1 j ■ I 1 i i ■ ................ I . 11111 j-1 I I . | ! 10 20 30 40 50 60 70 80 #716: Ethanamine, 2-(ethylthio)-, hydrochloride 90 100 110 120 130 140 MWMMAMAMWJAAk 3b 1 1 i ■ ' ' ' i ' ■ 1 1 i 1-1 ' 1 I 1 ' 1 1 I 76 5.80 6.00 6.20 6.40 5000 m/z 83.00 6.09% 38 47 61 105 15 All.. |l mllir ' - 4ITT 89 A 1 1 ' i ' ■' । ■'1 ■ ।1 ‘ I ’ । ■ 1 ■ ■ I ■ । ' । I । 1 1 ' I ■ /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #7641: 2-Propen-1 -ol, 2-chloro-, acetate ayaiMm,) npal, 43 5.80 6.00 16.20 6.40 m/z 84.00 5.90% 5000 99

57 15 29 .......... '' 1 1 1 , 111 36 ! +90—4 1.65 7^' 82 . 92 I I I I ( “f i l l ( I I I I I I I 106 116 ■ ।1 ■111111 ■ । 134 '1 ■ ।' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 5.80 6.00 6.20 6.40

10699.D SCAN020507 .M Wed May 15 08:36:12 2002 Page 4

NYC-WTC_000045728

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NYC-WTC_000045728Source: NYC Law Department, mirrored locally

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GCMS sample analysis results for AE10698, May 20 2002 · Box DEP Box 25

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Laboratory report detailing GC/MS analysis of sample AE10698 including surrogate recovery data in May 2002.

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