GCMS analysis results for sample AE10066, May 2002

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Laboratory report documenting GCMS analysis of sample AE10066 conducted on May 14, 2002, including surrogate recovery data.

NYC-WTC_000044215–000044226

Folder label: “GCMS X 4/26/02 A 5/8/02”

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NYC 9/11 Public Portal Document

’Data File C:\MSDCHEM\l\DATA\020507\10066.D Vial : 26 Acq On 8 May 2002 12:45 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 6.12 0.62 ug/1 44688 1,4-Dichlorobenzene-d4 11.37

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 64 2 5-Acetoxytridecane 242 C15H30O2 1000245-61-5 38 3 Undecanal 170 C11H220 000112-44-7 16 4 N-Cyclooct-4-enylacetamide 167 C10H17NO 1000191-08-6 9 Abundance Scan 517 (6.117 min): 10066.D (-512) (-) m/ z 43.10 100.00% 43

5000

' ' ' i 1 ' ' 1 i 1 1 ' ' I 1 1 ' 'T ' 1 1 1 I . 82 97 125 5.80 6.00 6.20 6.40 ....... 14 60...m , 1112, I'...... ■ ■ । 1 ■ । ■ । > । । । | 1 ‘ I 1 । । । । । , । ‘I ii । । । । । 221 m/z 125.00 9.51% m/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #3877: 2-Propanone, 1,1,1 -trichloro- 43

5000 '..... M........... A............ ‘‘‘I‘ ■ ■ । ■ Tt iiii r । । । IT 5.80 6.00 6.20 6.40 m/z 97.00 9.29% 15 J 27 ,53 63 73 83 97 110 125................ 1r' Ir" 1 1 1 ■ I ' ' ■ 1 i 1 .,. । । । । । । , . । । । । । । । । । । । i-|-i 'i । । । । । । । । । । 11 i 1 n/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #4231:5-Acetoxytridecane 43 AA I 'MA, 5.80 6.00 6.20 6.40 5000 m/z 47.00 7.79%

.... t" 55 69 83 97 111 129 ■Illi ■ ■ III ... I, I .I______________________ 1 82 I_____________________ MMwWMMVwMWWM Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #109568: Undecanal ' ' ' ........... | I I I ! | I >> I | 43 57 5.80 6.00 6.20 6.40 m/z 82.00 7.69% 82 5000 68 96 . 126 110 | . ...... Il. I ‘)11‘ "tk I" , I,'“.I ,||,’I ,I 1142152 -- I l Il, [ ,170................... I 1 1 I I -Terd I I < I I I I I I I I I I I AAAAAAALA , Al A , 1 । ' 1 ■ ■ । ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 5.80 6.00 6.20 6.40

10066.D SCAN020507 .M Tue May 14 08:47:00 2002 Page 3

NYC-WTC_000044222

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NYC-WTC_000044222Source: NYC Law Department, mirrored locally

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