GCMS analysis results for sample AE08964, May 7, 2002

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Laboratory report documenting GCMS analysis of sample AE08964 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000049622–000049633

Folder label: “GCMS X 4/16/02 A 4/24/02”

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NYC 9/11 Public Portal Document

'Data File : C:\MSDCHEM\1\DATA\020424\08964.D Vial: 15 Acq On : 24 Apr 2002 11:37 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************* ************************************************ Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.13 0.29 ug/1 343222 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 42 2 Butane, 2,2,3,3-tetranitro- 238 C4H6N4O8 020919-97-5 9 3 Butanoic acid, 2-acetyl-3-methyl... 158 C8H14O3 051756-10-6 9 4 2-Propanone, 1,1-dichloro- 126 C3H4C12O 000513-88-2 9 Abundance Scan 519 (6.129 min): 08964.D (-512) (-) m/z 43.10 100.00% 43

5000

’I’8’ . । ri . ’I’*I-*4I 5.80 6.00 6.20 6.40

miz-> 1...10....... . ,51 61 73 83 97.... 117125............. r.I । , > . . । . ..>। . ..,।III.।,,..j.,.i,.. ’ t . 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 । ■ ... । .... । . . । । । . . m/Z 42:1014:28% Abundance #3877:2-Propanone, 1,1,1-trichloro- 43

5000 ■ ■ i ■ ■ ‘ ■ i • ■ ■ ■ i ■ ■ • • । ■ i 5.80 6.00 6.20 6.40 m/z 124.90 7.54% 15

miz—> ml 27 35 10 27 36 HTHm’rr , 53 63 20 30 40 50 60 70 +73.741 90 97100 110117120125130 140 150 160 80 ' I • • “i • । •ji FE11111111111111

Abundance #3995: Butane, 2,2,3,3-tetranitro- 30 43 • • i • • • < i • ■• ’i. i । । । । ji। । 5.80 6.00 6.20 6.40 5000 m/z 83.00 6.76% 53 15 mH —1,1 |l,l|.........69........ 86.......................................................... miz-> 10 20 30 40 50 60 70 80 M 100 110 120 130 140 150 160 Abundance #7755: Butanoic acid, 2-acetyl-3-methyI-, methyl ester 40 । । Timp Aipii । TTmminnp 43 5.80 6.00 6.20 6.40 m/z 127.00 5.81% 101 5000 116 15 69

.7.1.51,59 27 84 127 . . *’nrt 11 n r >T> i । 1 > | i n rl i ■ TI’,1 . i. “t i 11।।। 143 158 I I J » I I . ■ ■ i • • • ■ i ■ • • 1 । ■ ■ > ■ । । । । । । iz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 5.80 6.00 6.20 6.40

08964.D SCAN020424.M Thu May 02 14:52:59 2002 Page 4

NYC-WTC_000049629

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NYC-WTC_000049629Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE08960, May 7, 2002 · Box DEP Box 27

NYC-WTC_000049571

Laboratory report documenting GCMS analysis of sample AE08960 conducted on May 7, 2002, by analyst DLV.

1 shared topics · Same agency, volume and box · similarity 0.998