GCMS analysis results for sample AE09153, May 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\020424\09152.D Vial: 21 Acq On : 25 Apr 2002 5:30 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.12 0.82 ug/1 1014300 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 38 2 Sulfurous acid, dipropyl ester 166 C6H14O3S 000623-98-3 9 3 Xylose 150 C5H10O5 000058-86-6 9 4 1,2-Ethanediol, monoacetate 104 C4H803 000542-59-6 9 Abundance Scan 518 (6.123 min): 09152.D (-510) (-) m/ z 43.10 100.00% 43

73 5000

' 1 1 1 ' ■ ' 1 1 1 1 ' 1 I ' 1 ........ I 83 99 ' I. 53 61 117125 5.80 6.00 6.20 6.40 35. -TTT TTTuOmgtTp m/z 73.10 53.39% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #3877: 2-Propanone, 1,1,1-trichloro- 43

5000 *Tun 5.80 6.00 6.20 6.40 m/ z 40.10 11.09% 152736 +50.63 TTHp+ 76 83 97 ' i ’ ■' ■ i11' • 1 ■1 ■ ''111 ■ ■ । 110117 125 ।।।। • ddl ■ ■ m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #109140: Sulfurous acid, dipropyl ester 43 5.80 6.00 6.20 6.40 5000 m/z 45.10 8.34% 27

..... 14,159, 59 66 73— 83dndunE-muOa"wTTT 95 107115 125 137 11101011 000’ n/z-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 #25780: Xylose 73 A-A-+4A4-4— 454 5.80 6.00 6.20 6.40 60 m/ z 41.10 8.21% 5000 43

h 86 । 97 105112119 133 150 n/z—> all 1 1 l ' ' ' 1 i r' 1 1 I ' 1 1 ' 1 1 ' r 1 1 1 1 ''' 1 ' "lf’ > ' 1 । 111 । । «« i r । । । । । । । i । । । i-i । । । । । । । । 1TnImm—RRTT 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 5.80 6.00 6.20 6.40

09152.D SCAN020424.M Fri May 03 10:59:23 2002 Page 4

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