GCMS analysis results for sample AE09153, May 2002

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Data File : C:\MSDCHEM\l\DATA\020424\09152.D Vial: 21 Acq On : 25 Apr 2002 5:30 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 8

R.T. EstConc . Area Relative to ISTD R.T.

3.65 0.21 ug/1 257588 1,4-Dichlorobenzene-d4 11.38

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 28 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 16 3 Thiirane, methyl- 74 C3H6S 001072-43-1 5 4 Urea, methyl- 74 C2H6N20 000598-50-5 4 Abundance Scan 98 (3.655 min): 09152.D (-94) (-) m/ z 74.00 100.00% 40 74 ____ ________ 82 5000 47 । i ! i . i-1-1- iiii |L । 1 1 i ■ '

m/z->10 20 30 L l-|‘l । । --P 40 50 60 70 58 vn 80 1 ' i ' ■ ■ r i ■ ' ■ ' i ' ■ ' ' i

90 100 110 340 3.60 3.80 4.00

Abundance #28338: Acetonitrile, dichloro- 74

5000 82 47 3.40 3.60 3.80 4.00 m/z 82.00 63.83% 35

/z-> .12... 2,1—11 .6062.........70 । 10 20 30 40 50 ’ l 1 1 1 • i ' 80 ■n-1 . 90 100 108 110 Abundance #115342: Acetonitrile, dichloro- 74 35 ,V|/Ka4+1 A| I 3.40 3.60 3.80 4.00 5000 82 m/z 75.90 30.72% 47

> ■ i ■ ■ • • i > ■ 1 ■ i > ■ 1 Pil...... I..... 1 TTI 1 1 । ■ r ■ । ' r 1 ' । ■ 1 । /z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115343: Thirane, methyl- MM... 4|1 74 3.40 3.60 3.80 4.00 m/z 84.00 29.21% 5000

47 vPhpoA 27 33 . ---33l+ 153.58.46841 11 ■ i । । 1 ■ । । । 1 1 1 ■ ■ ■ i । m/z-> 10 20 30 40 50 60 70 80 90 100 110 3.40 3.60 3.80 4.00

09152.D SCAN020424.M Fri May 03 10:59:21 2002 Page 3

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