GCMS analysis results for sample AE08964, May 7, 2002

NYC 9/11 Public Portal Document

'Data File : C:\MSDCHEM\1\DATA\020424\08964.D Vial: 15 Acq On : 24 Apr 2002 11:37 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Methane, dibromochloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 5.09 0.42 ug/1 502953 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methane, dibromochloro- 206 CHBr2Cl 000124-48-1 91 2 Methane, dibromochloro- 206 CHBr2Cl 000124-48-1 76 3 Methane, dibromochloro- 206 CHBr2Cl 000124-48-1 55 4 Cycloprop[a]indene, 6-bromo-1,la. .. 208 C10H9Br 055780-41-1 25 Abundance Scan 342 (5.089 min): 08964.D (-329) (-) m/z 128.90 100.00% 129

5000

■ ■ ' i ■ ' ' ■ i ■ • • ■ i ’ ' ' r I 1 ' 1 ' 48 35 ।, 81 93 160 173 208 4.80 5.00 5.20 5.40 ■ ■ i ■ ■ J‘ 1J____ ________ LLJ___ < > I > l . . I I > r < I . . , I I . I j . I . . ■ > i > > । * 11 •* l ■ • । m/z 126.90 85.80% miz-> 20 40 60 80 100 120 140 160 180 200 Abundance #121837: Methane, dibromochloro- 129

5000 TTMMMr 4.80 5.00 5.20 5.40 m/z 130.90• 25.18% 208 —48 _ 79 93 miz-> -36, 20 40 60 80 100 120 ....160 1/3...... ,h ■ i ■ ■ ■ • I ■ • 1 ■ i ■ • ■ ■ i ' 1 1 ' i 140 160 180 200 Abundance #121838: Methane, dibromochloro- 129 mm 4.80 5.00 5.20 5.40 5000 m/z 48.05 16.32%

48 79 93 138. ........ h 116 II 160 173 PtP 208 mfe-> Abundance 20 40 60 80 100 120 140 #57730: Methane, dibromochloro- 127 160 180 200 MhMAwvdMWvtn 4.80 5.00 5.20 5.40 m/z 40.10 15.24% 5000

48 79 91

/z—> 13 20 35 |L 40 64 II I 103 116 * « i * ' * 1 r* 60 80 100 120 11119 173,...1/30., 140 160 180 200 ' ' i • ‘ ■ ■ i ■ ‘ ' ■ i ‘ ' ■ ■ i ■ • 4.80 5.00 5.20 5.40

08964.D SCAN020424.M Thu May 02 14:52:57 2002 Page 3

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