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GCMS surrogate recovery results for sample AE00280, Jan 2002

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Laboratory record documenting GCMS surrogate recovery data for sample AE00280 analyzed on January 10, 2002.

NYC-WTC_000050893–000050911

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050908
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NYC 9/11 Public Portal Document

Data File : C : \MSDCHEM\1\5973N\02JAN09\280 . D Vial: 5 Acq On 9 Jan 2002 9:31 pm Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 9 N-perdeuteriobenzylideneani ... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.16 ug/L 136771 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 2 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 4 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 Abundance Scan 1656 (22.280 min): 280.D (-) m/z 192.10 100.00% 1912

5000 m.... . 22.00 22.20 22.40 22.60

mlz~> 0 .. 42.,.... ze.22.,*.. ,120... 146.150.... 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 191.10 15.29% Abundance #88409: N-perdeuteriobenzylideneaniline 192

5000 82 22.00 22.20 22.40 22.60 54 110 m/z96.00 15.08% 0 30 H 1 94 160 "I......................... I......I........... I' Trmm A 'I........... I i ■ i mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192 TU ■ ■ i 22.00 22.20 22.40 22.60 5000 m/z 146.10 12.87%

96 164

nlz-> 0 i ■ " ■ r ■ ■11 ■ ■ ■ ■ i" " r "' i A । ■i•■■•। 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 138 • 11 ■" ■ i X 4. Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene - 192 22.00 22.20 22.40 22.60 m/z 193.10 12.12%

5000

96 1 EE

n/z--> 0 WII“9n90"n9"na——nupnam—mmup9nnu*unnnuh 88 J 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 139 152 ,| 176 , U 22.00 22.20 22.40 22.60

280.D SCAN508.M Thu Jan 10 11:51:55 2002 Page 11

NYC-WTC_000050908

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NYC-WTC_000050908Source: NYC Law Department, mirrored locally

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