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← Document results/DEP Box 28/GCMS X 1/11/02 A 2/7/02
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GCMS blank results for sample AE00842, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS blank analysis of sample AE00842 with compounds below detection limits.

NYC-WTC_000052233–000052250

Folder label: “GCMS X 1/11/02 A 2/7/02

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Scanned page image, NYC-WTC_000052247
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB07\0111BA.D Vial: 1 Acq On : 7 Feb 2002 11:02 am Operator: Sample : lab blank 1/lla Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 10 N-perdeuteriobenzylideneani ... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.13 ug/L 79333 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 2 2-CYANOCARBAZOLE $$ 9H-Carbazole. . . 192 C13H8N2 057955-18-7 50 3 N- (2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 49 4 Bitoscanate 192 C8H4N2S2 004044-65-9 45 Abundance Scan 1656 (22.280 min): 0111 BA.D (-) m/z 192.10 100.00% 192 J 5000

146 senjvnnv ।1111 r1 * 160 0 49 1 ■ i ■' ■ ■ i11 ■ ■ i ■ ■ ■' i' 70 82 86 -HPPT HH 120 J 22.00 22.20 22.40 22.60 m/z 146.10 18.82% y/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192

5000 82 A.......... / i 1 ’ ■ 1 r1 ■ 1 1 । ■ ■ 22.00 22.20 22.40 22.60 54 m/z 193.20 17.61% 110 30 160 1 94 - 0 ■" ■ I" ■ ■ ।1 ■111 ■ i " 11 r 11' I'1" I "I'.............. 1 " i" " i ■ /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103420: 2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192

22.00 22.20 22.40 22.60 5000 m/z 191.10 16.93%

0 96 138 ■ ‘ 11" ' I " '' i " " r ’ " r 1" i " " r ■ ’' i' " ' i ■' " i " '' i' " ''I ■ " ' i1" ' r T111" ' i " " I । 11’1 /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 192 22.00 22.20 22.40 22.60 77 151 m/z 96.10 14.25% 130 5000 93 104 119

177 0 ■ i ■ I ■ 11 ' 11 .' 11............ I. " ' I"' * I' ’ ‘' I" " I Trmm ' i ■ ■ ■ ■ t •■ ■ ■ i ■ ■ ‘ I ■ " ■ । ‘ i" TITT TTyr 11 I 1 'T 1 1 1 ' r 1 ' I1 ' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

0111BA.D HP020702.M Thu Feb 21 09:58:24 2002 Page 12

NYC-WTC_000052247

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NYC-WTC_000052247Source: NYC Law Department, mirrored locally

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