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← Document results/DEP Box 28/GCMS X 1/9/02 A 1/15/02
Document / 11 pages

GCMS blank analysis for sample AE00365, Jan-Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS blank analysis results for sample AE00365 conducted between January 15 and 16, 2002.

NYC-WTC_000051674–000051684

Folder label: “GCMS X 1/9/02 A 1/15/02

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Scanned page image, NYC-WTC_000051682
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\0109B.D Vial: 1 Acq On : 15 Jan 2002 10:12 am Operator: Sample : lab blank 1/9 Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 4 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.12 ug/L 60651 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 72 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 3 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 52 4 1-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 083415-88-7 50 Abundance Scan 1656 (22.280 min): 0109B.D (-) m/z 192.10 100.00% 192

5000 -- 96 146 82 160 22.00 22.20 22.40 22.60 40 66 — 0 T Frit I MIT’ I I > | I | | | | I I r '111 ■ ■' ■ i • ■ ■ ■ i''' ■ i ■ ■ ‘T . .................. I T" "z 96.10 17.92% nz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 ' 1 1 1 1 ' 1 1 11 ’ 1 I1 1 ' 1 T 1 1 22.00 22.20 22.40 22.60 96 164 m/z 146.10 16.78% 138 Ok * I,.......... 11, ---T 11111'11111111"4-rrym m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 .... A ' ' I ' ' ' ' I ' ' ' ' I ' 22.00 22.20 22.40 22.60 5000 m/z 193.10 15.45%

96 165 139 152 176 , . 88,11. ok ■ ।■111 ■1' । ■ "'I " " 111 ” I TITTTTT 111'' 111 " I — Tumm n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 192 1 I " " I । L 22.00 22.20 22.40 22.60 77 151 m/z 191.10 15.09% 130 93 104 5000 119

177 ok " r " ' i " 111 " " I ‘TTII ‘ ‘‘I TITT TT’T TTIT , I....... I ' i' " ‘ i " " i " " i " 1..... 111111' ' 1 1 1 ' ......... 1 /z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

O109B.D SCAN508.M Wed Jan 16 08:14:17 2002 Page 6

NYC-WTC_000051682

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NYC-WTC_000051682Source: NYC Law Department, mirrored locally

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