GCMS results for sample AE00561, Jan 17 2002

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GCMS analysis log for sample AE00561 showing surrogate recovery and unknown compounds detected on January 17, 2002.

NYC-WTC_000051755–000051767

Folder label: “GCMS X 1/9/02 A 1/15/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00561.D Vial: 5 Acq On : 15 Jan 2002 4:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 66653 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 72 2 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 72 3 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H1203 000607-91-0 64 4 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 52 Abundance Scan 1656 (22.280 min): 00561 D (-) m/z 192.10 100.00% 192

5000

96 146 82 22.00 22.20 22.40 22.60 0 44 70 ..... I...... । ■1 ■ ।11111 .. ........ .............. Il m/z 96.00 17.32% n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 1 70 180 190 200 | Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 22.00 22.20 22.40 22.60 96 164 m/z 193.10 15.44% I 138 / 0 —PPPPPTTITT T’TT m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103420: 2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192

22.00 22.20 22.40 22.60 5000 m/z 146.10 15.29%

m/z-> Of ' i • ‘' i' ■'' ir ..... 96 .........138 ... X,..... I. 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TTU’

Abundance #102624:1,3-Benzodioxole, 4-methoxy-6-(2-propenyl)- (CAS)... . ............. 0................. 192 22.00 22.20 22.40 22.60 m/z 191.10 13.34% 5000

91 165

0 • ।' ■' ■ i ■ ■ ■ ■ i ■ ■ ■' i ■ .. .1103 ′′′ 1111' * 11''11 119 I 131 II '' I ’1' ’ I " 147 I I' ■ ■' i 1177 ■ I'' " 11 1 ‘11 ’'1' T’I’ Tru ‘""f /z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

30561.D SCAN508.M Wed Jan 16 08:14:14 2002 Page 7

NYC-WTC_000051765

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NYC-WTC_000051727

Laboratory report showing GCMS analysis results for sample AE00559 conducted on January 17, 2002.

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