Gas chromatography-mass spectrometry analysis of sample AE00738 conducted on 1/29/02, detecting unknown compounds and 2,4-DDD surrogate at 99 ug with 5.0 MDL.
NYC-WTC_000051948–000051966Folder label: “GCMS X 1/10/02 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\1\5973N\02JAN16\00738.D Vial: 6 . Acq On : 16 Jan 2002 7:17 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 11
R.T. EstConc Area Relative to ISTD R.T.
22.28 0.15 ug/L 90421 Phenanthrene-dl0 22.63
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Cyanocarbazole $$ 9H-Carbazole ... 192 C13H8N2 057102-93-9 59 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 3 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 49 4 2-Imidazolidinone, 1-methoxy-3-p... 192 C10H12N2O2 052420-43-6 47 Abundance Scan 1656 (22.280 min): 00738.D (-) m/z 192.10 100.00% 192
5000 ........................ ........ 96 146 160 82 22.00 22.20 22.40 22.60
n/z-> 0 +49 120 66 a.. I.... . ' ■ ■ r ' ■ ■ । । । । i'| । । । । । । । I । । 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 96.10 17.36% Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192
5000 22.00 22.20 22.40 22.60 96 164 m/z 146.10 16.00% 138 0 ■ ■ i " ■' i1 ■' • i ■ ■1 ■ i ■' ■11' ■ ■ ■ i'1' ‘ 11' ' i"1 ■ i1 •" i ‘1 ■11111 h1 ■ ■ ■ ।.' ■' ।1 I 1 1 " I 1 r L m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 -AP 22.00 22.20 22.40 22.60 5000 82 m/z 191.10 15.93%
54 110
m/z—> 30 0 " 11 i11" 11" ' 11 1 1 1 "1 ' I 1 1 1 1 1 94 | mll... I" 160 '1 r " ■ r ■ " i1 ’ ■ ■ । ■ T TTTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 I Abundance #102494: N-(2-methylpro|>2-enyl)-2-nitrobenzenamine 192 22.00 22.20 22.40 22.60 77 151 m/z 193.00 14.85% 130 93 104 5000 119
177 0 TTTCTTTTT r ■" ।" "i" " । "1 r TTTrr T’T TTTr TrTm /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 2240 22.60
10738.D SCAN508.M Thu Jan 17 08:17:47 2002 Page 10
NYC-WTC_000051961
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NYC-WTC_000051860
GCMS analysis log for sample AE00697 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051895
GCMS analysis log for sample AE00702 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051877
GCMS analysis log for sample AE00701 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051697
Laboratory report showing GCMS analysis results for sample AE00470 conducted on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051549
Laboratory report showing GCMS analysis results for sample AE00556 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052291
Laboratory report detailing GCMS scan results for sample AE00844, including detection of unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052311
Laboratory report detailing GCMS scan results for sample AE00841, including detection of unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000051782
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051783
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 10 and 16, 2002.
Filed in the same folder
NYC-WTC_000051785
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051789
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051794
GCMS analysis log for sample AE00703 showing blank results with compounds below detection limits on January 16, 2002.
Filed in the same folder