GCMS results for sample AE00557, Jan 17 2002

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GCMS analysis log for sample AE00557 showing surrogate recovery and unknown compounds detected on January 17, 2002.

NYC-WTC_000051768–000051781

Folder label: “GCMS X 1/9/02 A 1/15/02”

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NYC 9/11 Public Portal Document

Data File : C : \MSDCHEM\1\5973N\02JAN15\00557 . D Vial: 1 Acq Cn : 15 Jan 2002 1:32 pm Operator: . Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L *********************************************************** ********** Peak Number 6 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.14 ug/L 83471 Phenanthrene-diO 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 59 2 N-perdeut er iobenzyl ideneani line 192 C13D11N 000538-51-2 52 3 l-amino-2-methyl-4-isopropyl-thi ... 192 C5H13N4PS 107264-54-0 50 4 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 49 Abundance Scan 1656 (22.280 min): 00557. D (-) m/z 192.10 100.00% 192

5000

' ' I ' ' ' ' I 1

49 70 82 %6 118 T 160 'I " " I' " 1111'1 rr 11111111111111111111111111111111 (11 22.00 22.20 22.40 22.60 m/z 96.00 14.69% 0 TTPTTTTTT 11" " 11"11 /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424: 3-Cyanocarbazole $$ 9H-Carba2ole-3-carbonitrile (CAS 102

5000 ... . ....ft 22.00 22.20 22.40 22.60 m/z 191.00 14.54% 96 164 0 TIT —TmmPT 1.......... 11, 1'I " '' 111 " 111 T’i | 138 1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 102

22.00 22.20 22.40 22.60 5000 82 m/z 193.10 14.28%

54 110 30 94 160 0 —PTTTTTT " i " " i ■' " i -HP TTTTTT TImn m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin... 159 102 22.00 22.20 22.40 22.60 m/z 146.10 11.60%

5000

144 177 0 i "'' r ''' i " " i " " i L i' " ' r " ' i " ■ ■ i " '' i " " i m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TETTt i i I i ! II I A r I ri n / i \ I I

22.00 22.20 22.40 22.60

00557.D SCAN508.M Wed Jan 16 08:13:57 2002 Page 8

NYC-WTC_000051779

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