GCMS results for sample AE00557, Jan 17 2002

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GCMS analysis log for sample AE00557 showing surrogate recovery and unknown compounds detected on January 17, 2002.

NYC-WTC_000051768–000051781

Folder label: “GCMS X 1/9/02 A 1/15/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\O2 JAN15\00557.D Vial: 1 Acq On : 15 Jan 2002 1:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Benzene, methoxy- (CAS) $$ ... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 18.43 0.11 ug/L 59356 Acenaphthene-diO 18.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene, methoxy- (CAS) $$ Aniso... 108 C7H80 000100-66-3 9 O 2 Benzene, methoxy- (CAS) $$ Aniso... 108 C7H8O 000100-66-3 7 3 Benzene, methoxy- $$ Anisole $$ ... 108 C7H80 000100-66-3 5 aneCou 4 Ethanol, 2-(3-methylphenoxy)- $$... 152 C9H12O2 013605-19-1 5 Abundance Scan 1319 (18.433 min): 00557.D (-) m/z 57.10 100.00% 57

71 108 5000 65 138 41 84 154

92 18.00 18.20 18.40 18.60 18.80

n/z-> 01T——Tm : 30 40 50 60 49 J....i.IL,i. 70 100 110 120 130 140 150 80 90 i • ■ ■ ■ । ■ i ■ ■ i 1 111 i 160 m/ Z 71.10 57.37% Abundance #11332: Benzene, methoxy- (CAS) $$ Anisole $$ Anisol $$ An... 108 65 78 5000 39 1 I'1 ' 18.00 18.20 18.40 18.60 18.80 51 93 rn/z 108.10 53.91% 01 i ■ ■ ■ ■ i ■ 1 1 1 । 1 1 1 1 ' | i ■ • 1 ' i 1 ' ■ ■ i ■ ■ m/z-> ;30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #11334: Benzene, methoxy- (CAS) $$ Anisole $$ Anisol $$ An... 108 65 I 1 1 1 1 1 1 1/1 11Pu fr I । । । 1 I । 1 78 18.00 18.20 18.40 18.60 18.80 5000 39 m/z 65.00 47.98% 51 93 olTIT --- TT-T-r-r-j-rS-r-r-p-r m/z--> :30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #11338: Benzene, methoxy- $$ Anisole $$ Anizol $$ Methoxyb... I 11 ■ 1 | ■ > 1 I’I* I ' ' i ' ' 108 18.00 18.20 18.40 18.60 18.80 65 78 m/z 138.10 46.13%

5000

51 93 38 — 0 + i r ' 1 ' i ‘ ■ 1 i 1 ■ i 111'' ।111111111111111111111 m/z—> 30 40 50 70 80 90 100 110 120 130 140 150 160 18.00 18.20 18.40 18.60 18.80

00557.D SCAN508.M Wed Jan 16 08:13:57 2002 Page 7

NYC-WTC_000051778

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