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GCMS blank analysis results, Feb 25-26 2002

Machine-extracted title · confidence 90%

Laboratory report showing GC/MS analysis results for a blank sample testing specific compounds on February 25 and 26, 2002.

NYC-WTC_000003425–000003443

Folder label: “GCMS X 1/20/02 A 2/25/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\0116B.D Vial: 1 Acq On : 25 Feb 2002 11:14 am Operator: ' Sample : lab blank 1/16 Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 (1,1,1,3,3,3-hexadeuterio)-... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T. 6.58 0.04 ug/L 12132 1,4-Dichlorobenzene-d4 9.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 (1,1,1,3,3,3-hexadeuterio)-aceto... 106C5H6D6N2 123499-00-3 4 2 Benzene, ethyl- (CAS) $$ EB $$ E... 106 C8H10 000100-41-4 4 3 Ethylbenzene $$ Benzene, ethyl- ... 106 C8H10 000100-41-4 4 4 Benzene, ethyl- (CAS) $$ EB $$ E... 106 C8H10 000100-41-4 4 Abundance Scan 284 (6.580 min): 0116B.D (-) m/z 91.00 100.00% 91 A A 106 5000

51 ——

,............................................... 84 6.20 6.40 6.60 6.80 7.00 0 •' i"' ■ i ■" ■ i' • ■ i ■" ■ i ■ • " i ■ ■ ■ ■ i' m/z 106.10 60.32% mfz~> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 Abundance #8157: (1,1,1,3,3,3-hexadeuterio)-acetone N,N-dimethylhydr... 106

44 5000 T-r-p-r-r-r-j-r- 6.20 6.40 6.60 6.80 7.00 61 m/z 50.90 19.24% 40 . 48 0 mH TITTT ■11" i ■"■ i"■ ■ i■ ■ ■ ■ i■ ■ “i “ "i ■ ■ ■ ■ i'■ ■ ■ ■ i ■ ■' ■ i ‘ mfz-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 Abundance #10718: Benzene, ethyl- (CAS) $$ EB $$ Ethylbenzene $$ Phe... 91 6.20 6.40 6.60 6.80 7.00 5000 m/z 105.00 19.13% 106 j 51 65 77 0- ■' i “1 ■ i ■ “ 111 “11 mmmmmmmH Immmmmmmm m/z—> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 Abundance #10714: Ethylbenzene $$ Benzene, ethyl- $$ Ethylbenzol $$ ... 91 ■ i ■ ■ ■ ■ i ■ ' 6.20 6.40 6.60 6.80 7.00 m/z 49.00 2.89%

5000- 106 "MWMMAWWp/ 51 65 77

m/z—> 0 p 3035404550556065 70 75 80 85 90 -H laglagong 95 100 105 110 115 6.20 6.40 6.60 6.80 7.00

116B.D HP022102.M Tue Feb 26 08:30:42 2002 Page 9

NYC-WTC_000003436

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NYC-WTC_000003436Source: NYC Law Department, mirrored locally

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