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← Document results/DEP Box 12/GCMS X 1/20/02 A 2/25/02
Document / 19 pages

GCMS blank analysis results, Feb 25-26 2002

Machine-extracted title · confidence 90%

Laboratory report showing GC/MS analysis results for a blank sample testing specific compounds on February 25 and 26, 2002.

NYC-WTC_000003425–000003443

Folder label: “GCMS X 1/20/02 A 2/25/02

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Scanned page image, NYC-WTC_000003435
OCR text

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\0116B.D Vial: 1 Ac'q On : 25 Feb 2002 11:14 am Operator: ' Sample : lab blank 1/16 Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 3-(CYCLOHEX-3’-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.96 0.32 ug/L 104049 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 4 N^-DIMETHYL-2-BUTOXYISOPROPYLAMINE 159 C9H21NO 000000-00-0 9 Abundance Scan 229 (5.959 min): 0116B.D (-) m/ z 73.00 100.00% 73

5000

43 ■ 1 i 1 ■ ■ ■ i ‘ ■ i ■ ' ■ ■ i 5.60 5.80 6.00 6.20 6.40 0- i ——1B9ngnmm]Pmmmpmp 1111 97 m/z 43.00 19.51% niz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 ■ ■ i • 5.60 5.80 6.00 6.20 6.40 43 m/z 45.10 10.43% 27 55 87..... ................... . 0- 1 I ' • i ■ ‘ • ■ i'1 1 ■ ' i ■ “ ' i " ‘ 'T't H miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3dioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 ‘ 6.20 6.40 5000 m/z 41.10 9.76% 43 27 55 87 113 174 A 0--TTt ■ i ■ ■ ■ ■ i ■" ■ T • Hr 1thji' ■1 ■ i ■ ■ “ i i ■ ■ ■■ i" “ i ■ ■ ■ ■ i “ ■ ■ i ■■ ■ ■ i ■11 ■ i' miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9663:3-Pentanol, 3-methyl- • ■ i ■ • ‘ 1 I ' ■ ■ ■ i ■ ■ i ■ ‘ ■ i ' 73 5.60 5.80 6.00 6.20 6.40 m/z 74.10 6.24% 5000 55 27 45 87 0 ‘ I ’ ' ′′ ! ‘ ‘ ‘ I ‘ ‘ ’ * I • T Tmmmmmmmmpp ' 11 ■ ■1 ■ । ■ ■ • ■ • 1 1 I 1 ' 1 ‘ I 1 miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20 6.40

0116B.D HP022102.M Tue Feb 26 08:30:42 2002 Page 8

NYC-WTC_000003435

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NYC-WTC_000003435Source: NYC Law Department, mirrored locally

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GCMS analysis results, Feb 27 2002 · Box DEP Box 12

NYC-WTC_000003463

Gas chromatography-mass spectrometry results for sample AE01138 identifying unknown compounds and surrogates on February 27, 2002.

4 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991

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