Laboratory report showing GCMS blank analysis results for sample AE00365 conducted between January 15 and 16, 2002.
NYC-WTC_000051674–000051684Folder label: “GCMS X 1/9/02 A 1/15/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\1\5973N\02JAN15\0109B.D Vial: 1 Acq On : 15 Jan 2002 10:12 am Operator: ' Sample : lab blank 1/9 Inst : Instrumen Mise : January 15, 2002 Muitiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C: \DATABASE\WILEY7N. L ********************************************************************* Peak Number 3 3 -(CYCLOHEX-3'-EN-YL)PROPAN. .. Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
5.89 4.59 ug/L 1293740 1,4-Dichlorobenzene-d4 9.72
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 23 4 1,3-Dioxolane, 2-methyl- (CAS) $... 88 C4H802 000497-26-7 9 Abundance Scan 220 (5.885 min): 0109B.D (-) m/z 73.10 100.00% 73
5000 43 1 - t ■ ■ TrT 5.60 5.80 6.00 6.20 oW — 55... J , 87 103 1 11 1,1 111 1 'I' 11UTTIWWTI*TIWTTTWTWWWTTTTTWTTTTT)T m/z 43.10 24.29% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 7(3 "■-I _ _
5000 5.60 5.80 6.00 6.20 43 m/z 45.10 10.04% 27 OTTTT r 11 ■ r TT55‘ I’’’ 'I' + , I 87 113 174 i ■ " ■ r ■ ‘ ■ i ’ " 1 r ■'' i ■ " ■ i i11" r /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73
5.60 5.80 6.00 6.20 5000 m/ z 41.10 8.80%
43 27 55 ,i 87 113 174 0 " |11 " I 1 "''T ' । • |'I I' 1" i n ''' i" 111" I " I TWmuuummmeTum m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ................ . Abundance #4814: Silane, tetramethyl- " ' T ""I 1 ’ 73 5.60 5.80 6.00 6.20 m/z 71.10 6.10%
5000
m/z-> o ■■i■ 15 45 | j 53 • j । ■ ■ ■ । 1 ‘ 1 ' I I l’i • i . । । 88 T‘TE01mmauuuu*un 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ‘u01‘——TTT1 5.60 AT 5.80 L 6.00 6.20
0109B.D SCAN508.M Wed Jan 16 08:14:17 2002 Page 5
NYC-WTC_000051681
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NYC-WTC_000051794
GCMS analysis log for sample AE00703 showing blank results with compounds below detection limits on January 16, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050825
Blank analysis report for GCMS of sample AE00277 showing compounds below method detection limits from January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050716
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on January 25-February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050444
Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052233
Laboratory report showing GCMS blank analysis of sample AE00842 with compounds below detection limits.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050627
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on February 4-7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050893
Laboratory record documenting GCMS surrogate recovery data for sample AE00280 analyzed on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051624
Laboratory report showing GCMS analysis results for sample AE00615 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003425
Laboratory report showing GC/MS analysis results for a blank sample testing specific compounds on February 25 and 26, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000051662
Raw mass spectral data and abundance charts for sample AE00616 generated during analysis on February 1, 2002.
Filed in the same folder
NYC-WTC_000051663
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 9 and 15, 2002.
Filed in the same folder
NYC-WTC_000051665
Laboratory report showing GCMS calibration results for sample AE00365 conducted between January 15 and 16, 2002.
Filed in the same folder
NYC-WTC_000051669
Laboratory report showing GCMS reference analysis results for sample AE00365 conducted between January 15 and 16, 2002.
Filed in the same folder
NYC-WTC_000051685
Laboratory report showing GCMS analysis results for sample AE00365 conducted on January 17, 2002.
Filed in the same folder