Laboratory report showing GCMS blank analysis results for sample AE00365 conducted between January 15 and 16, 2002.
NYC-WTC_000051674–000051684Folder label: “GCMS X 1/9/02 A 1/15/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\1\5973N\02JAN15\0109B.D Vial: 1 Acq On 15 Jan 2002 :10:12 am Operator: Sample lab blank 1/9: Inst : Instrumen Mise January 15, 2002 : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L
Peak Number 2 Hexahydropyridine, 1-methyl... Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T. 5.51 0.10 ug/L 29357 1,4-Dichlorobenzene-d4 9.72
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Hexahydropyridine, 1-methyl-4-[4... 207 C12H17NO2 094427-47-1 74 2 cis-4-Ethoxy-b-methyl-b-nitrosty... 207 C11H13NO3 000000-00-0 64 3 2-(1'-METHYLINDOL-3'-YL)ETHENE-1... 207 C13H9N3 065037-75-4 5 4 Dodecahydropyrido[1,2-b]isoquino... 207 C13H21NO 000000-00-0 5 Abundance Scan 187 (5.509 min): 0109B.D (-) m/z 207.00 100.00% 207
40
5000
AAAAAAM. 5.20 5.40 5.60 5.80 49 0 TTp 1111" । । j .> I . । । . I 1 i f ... r | m/z 40.00 66.25% n/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 vAAMwu Abundance #125674: Hexahydropyridine, 1-methyl-4-[4,5-dihydroxyphenyl]- 207 70 42 97 5000 ndnmnDDnTEmT 82 5.20 5.40 5.60 5.80 136 m/z 208.00 27.27% 123 | 150 192 0 ‘‘I " i ■' ■ ■ i'r TTTOTTTTTTTLTTTTTTTTTTTTTTTTTTTTTITTTTTTTTT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #125417: cis-4-Ethoxy-b-methyl-b-nitrostyrene 160 207 ■ ■ ' । ■ i ■ । . . . . । । । 132 5.20 5.40 5.60 5.80 5000 77 m/z 49.00 3.34% 103 121
94 149 WAwuly/yphwd 0 i'' ■ ’ i l I - 11111' " 11 " '1111 " i " I /z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #125731: 2-(1'-METHYLINDOL-3‘-YL)ETHENE-1,1-DECARBONITRILE... 207 5.20 5.40 5.60 5.80
5000 165 62 88 138 179 101 112 . 152 192 0 * T’T . 1 .......................... ■II.. ,1... ■111 • ■ ■ । • T’T m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210
0109B.D SCAN508.M Wed Jan 16 08:14:17 2002 Page 4
NYC-WTC_000051680
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NYC-WTC_000051794
GCMS analysis log for sample AE00703 showing blank results with compounds below detection limits on January 16, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050825
Blank analysis report for GCMS of sample AE00277 showing compounds below method detection limits from January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050716
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on January 25-February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050444
Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052233
Laboratory report showing GCMS blank analysis of sample AE00842 with compounds below detection limits.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050627
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on February 4-7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050893
Laboratory record documenting GCMS surrogate recovery data for sample AE00280 analyzed on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051624
Laboratory report showing GCMS analysis results for sample AE00615 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003425
Laboratory report showing GC/MS analysis results for a blank sample testing specific compounds on February 25 and 26, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000051662
Raw mass spectral data and abundance charts for sample AE00616 generated during analysis on February 1, 2002.
Filed in the same folder
NYC-WTC_000051663
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 9 and 15, 2002.
Filed in the same folder
NYC-WTC_000051665
Laboratory report showing GCMS calibration results for sample AE00365 conducted between January 15 and 16, 2002.
Filed in the same folder
NYC-WTC_000051669
Laboratory report showing GCMS reference analysis results for sample AE00365 conducted between January 15 and 16, 2002.
Filed in the same folder
NYC-WTC_000051685
Laboratory report showing GCMS analysis results for sample AE00365 conducted on January 17, 2002.
Filed in the same folder