GCMS blank results for sample AE00842, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB07\0111BA.D Vial: 1 Acq On : 7 Feb 2002 11:02 am Operator: . Sample : lab blank 1/lla Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 3 2-hydroxymethyl -2,3,3-trime... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

6.07 0.15 ug/L 52732 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-hydroxymethyl-2,3,3-trimethyl-... 116 C6H12O2 110933-26-1 9 2 DEUTEROACETONE 59 C3H5DO 004468-52-4 5 3 3-Methylpyrrolidin-3-ol 101 C5H11NO 000000-00-0 5 4 Morpholine, 4-methyl- (CAS) $$ N... 101 C5H11NO 000109-02-4 5 Abundance Scan 236 (6.068 min): 0111 BA.D (-) m/z 43.10 100.00% 48

n/z-> 5000

0 49 ■ p n 1 IT I" ■11 59

84 I'''' I''' ■ I'' ■11 I ’ " ' P "' I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 101

m/z 5.80 II 6.00 59.10 6.20 m— A 6.40 61.16% Abundance #16765:2-hydroxymethyl-2,3,3-trimethyl-oxirane $$ Oxirane... 40 59

5000 5.80 6.00 6.20 6.40 31 m/z 58.00 27.31% 55 73 85 m/z-> 0 TIPTTTTT ..... rr 111111111111 • 111111111 rH I ■ ■' ■ I''111' *'11 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #587: DEUTEROACETONE 43

5.80 6.00 6.20 6.40 5000 59 m/z 101.10 27.20%

31 39 .

n/z-> 0 TPTTTTTHH .. Ill. l‘‘‘‘1‘171 ! > . . . । . . . . । . > i - ! . . . . । . nt । 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Tr

Abundance #8924:3-Methylpyrrolidin-3-ol 59 5.80 6.00 6.20 6.40 m/z 41.00 14.52% 42 5000 101

55

m/z-> 0 TIU’UII’IT ' I " •' 11 I' ‘‘ I'1 ’' I''-' I'''' 111' ’ I' ’111'''' I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 WTTTTTTT 5.80 A. 6.00 6.20 6.40

0111BA.D HP020702.M Thu Feb 21 09:58:23 2002 Page 5

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