GCMS blank results for sample AE00842, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\0111BA.D Vial: 1 Acq On : 7 Feb 2002 11:02 am Operator: . Sample : lab blank 1/lla Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

5.92 0.70 ug/L 239843 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 23-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 Pentanol, 5-amino-______________________ 103 C5H13NO 002508-29-4 9 Abundance Scan 223 (5.920 min): 0111 BA.D (-) m/z 73.10 100.00% 73

5000 43 ' 1 i 1 ■ ■ ' i ' ' 1 i' 1 ′ 1 i 5.60 5.80 6.00 6.20 ........... 1,117555... 1, ।.. 87... 103.......................... m/z 43.10 26.27%

W 01 "‘‘0‘‘C"UT"TTTTTTETTEIT ‘TT‘1‘T‘IT"II‘U11"11‘1117111T17 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 70

5000 4 ' ' I ' ' ' ' 1 1 '• ‘ I 5.60 5.80 6.00 6.20 43 m/z 41.10 9.51% 27 55 87 113 174 0'"I........... '.......... . ■ r ■ ■' i ■ ■ ■ ’I’ II i'' ■ ■ i' ■'' i ■ " ■ i' •'11 ■'' ■ i PTmg miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3‘-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 -1 1 ■ । AA ' 1 i 1 1 1 ' r' 1 1 ■ । ' 1 ' । 5 60 5.80 6.00 6.20 5000 m/z 45.10 9.39% 43 27 55 87 01 TPT 11" " i " ■ 'I1 Ipn 113 i'' ■' i " " r " ■ r ■ " r " ■ i" " i " " i ’' " i ‘1" 11 174 m/z~> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 30 -A 5.60 5.80 6.00 6.20 73 m/z 71.00 7.54% 5000 44 58

15 - 0 ' 'I"1'11" 1' r■"i'1" i " 1'i■ " 'i " ■■ i ■ " ' i " ' ■ i ■ " ' i' ■ ‘ ■ i' " ' i ‘1' ■ i' ■ ■ ■ i ‘ । > । । । •»'(■ > • i ■ • ■ • । ■ i /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 600 6.20

0111BA.D HP020702.M Thu Feb 21 09:58:23 2002 Page 4

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