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GCMS blank results for sample AE00842, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS blank analysis of sample AE00842 with compounds below detection limits.

NYC-WTC_000052233–000052250

Folder label: “GCMS X 1/11/02 A 2/7/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB07\0111BA.D Vial: 1 Acq On : 7 Feb 2002 11:02 am Operator: . Sample : lab blank 1/lla Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ***************************************************************** * * * * Peak Number 1 Butanoic acid, methyl ester Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

3.60 0.12 ug/L 42725 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butanoic acid, methyl ester 102 C5H10O2 000623-42-7 83 2 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 83 3 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 83 4 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 78 Abundance Scan 20 (3.602 min): 0111 BA.D (-) m/z 74.10 100.00% 43 7l4

5000 59 87 1 ■ ■ r ■ ■' ।11'111 f 1 ■ i'1 ■ ■ i ■11' i1 ■' ■ I 207 3.50 3.60 3.70 3.80 3.90 4.00 .7. |

m/z-> 0- orpo... TIT I""I""I""I'"11" "I" "11'•'i" "i" "i" "r"■ r"' i'" 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 m/z 43.10 93.30% Abundance #9218: Butanoic acid, methyl ester 43 74

5000 A 27 3.50 3.60 3.70 3.80 3.90 4.00 15 59 m/z 71.10 66.21% 87 102 0 i" " r 1" i" " i TTT Ipm " i" " i"1111 ■ "i" " i" "i" "i" "i" " i TF m/z--> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #9228: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43 74 mA 3.50 3.60 3.70 3.80 3.90 4.00 5000 m/z 41.10 36.21% 59 87

0- I....I .... 102 r1" । ■ i ' ■ ■ i ■' ■' i'1 ■' I I"111"1' i111' i" " I" " i" " r'" i" " i" " i" ‘' i" " I miz-> Abundance 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 #9222: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43 74 -A3.50 3.60 3.70 3.80 3.90 4.00 m/z 59.00 29.64% 5000 59 87

I|l.... 1... " i" ■11" "102 33 0 i■ • i ■■ ■■ i i1" ' i" ’' i''" i" " i''1111"' i" " i" " i" " 11"' i" " i'11 Tru. ।, 11,,, T T’ .. 11 rn/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 3.50 3.60 3.70 3.80 3.90 4.00

0111BA.D HP020702.M Thu Feb 21 09:58:23 2002 Page 3

NYC-WTC_000052238

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NYC-WTC_000052238Source: NYC Law Department, mirrored locally

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