GCMS blank analysis results, Feb 25-26 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB25\0116B.D Vial: 1 , Acq On : 25 Feb 2002 11:14 am Operator: Sample : lab blank 1/16 Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 9-Borabicyclo[3.3.1]nonane,... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

5.51 0.05 ug/L 16697 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 9-Borabicyclo[3.3.1]nonane, 9-[3... 207 C13H26BN 000000-00-0 5 2 Hexahydropyridine, l-methyl-4-[4... 207 C12H17NO2 094427-47-1 5 3 3-Methylindole-2-carboxylic acid... 207 C12H17NO2 000000-00-0 5 4 3,4-dihydro-6,7-dimethoxyisoquin. .. 207 C11H13NO3 084122-10-1 5 Abundance Scan 189 (5.507 min): 0116B.D (-) m/z 207.00 100.00% 2(7

5000 96 49 191 ■ • • ■ । • i ■ • • ' i ■ ■ ■ • i > • • ■ । 84 5.20 5.40 5.60 5.80 Ot 1′1—2217771197721111111729187 ■ i ■" • i ■ • “ i ■ ■ “ i “ ■ ■ i " i ■* “ i'1 “ i “ ■ ■ i “ i i ■' }t" m/z 208.00 36.91% niz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #125816:9-Borabicyclo[3.3.1]nonane, 9-[3-(dimethylamino)p... 58 150 2017 98

5000 70 111 124 ■ ■ ■ i ■ ■ ‘ ■ i ■ ' ' ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i

5.20 5.40 5.60 5.80 164 m/z 96.00 23.99% 192 Of ’’’1’1411’* i"" "••r “'i1' i ■ “ ■ i" " i ' ■ i •' “ i “ ■ ■ ’ ’’I’ 1 ■ i ■' •' i “ ■ ■ i1 ■ ■' i1' niz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #125674: Hexahydropyridine, 1-methyl-4-(4,5-dihydroxyphenyr|- 2017 70 42 97 5.20 5.40 5.60 5.80 ‘ ' i ■ • ■ ■ i ■ ' ■ ■ i • 1 ■ ■ i

5000 m/z 190.90 18.02% 82 136 150 192 0+ "’II I ■i■ • 123 ।....।....। । TIWTPTTTITTTTITTTTTT I’T mH niz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #125677:3-Methylindole-2-carboxylic acid, 4,5,6,7-tetrahy... • * r’ ’ * ‘ i * • » I * » < i r i rr I ) 207 5.20 5.40 5.60 5.80 133 m/z 49.00 13.65% 5000 77 105 162 179 My/Manopoo 49 151

•nfz~> 0 mm TPr 10101219.7/211 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 5.20 5.40 5.60 5.80 1

0116B.D HP022102.M Tue Feb 26 08:30:42 2002 Page 7

NYC-WTC_000003434