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GCMS analysis results for sample AE00613, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.

NYC-WTC_000051586–000051604

Folder label: “GCMS X 1/9/02 A 1/29/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN29\00613.D Vial: 2 - Acq On : 29 Jan 2002 3:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 3-Penten-2-ol (CAS) $$ 2-PE... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 5.71 0.11 ug/L 54797 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Penten-2-ol (CAS) $$ 2-PENTEN-... 86 C5H10O 001569-50-2 46 2 3-Penten-2-ol (CAS) $$ 2-PENTEN-... 86 C5H10O 001569-50-2 37 3 3 -[.beta.-hydroxy-(.beta.,.beta.... 86 C5H6D2O 005557-87-9 36 4 1-Trifluoroacetoxy-2-methylpentane 198 C8H13F3O2 000000-00-0 33 Abundance Scan 205 (5.714 min): 00613.D (-) m/z 41.10 100.00% 4h 71

5000 45 53 58 67 . 84 ---A5.40 5.60 5 80 6.00 — 1I011000000’00—’tlt 449—-H ■11" 1 ■ i'' 1..... m/ z 43.10 86.90% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4048: 3-Penten-2-ol (CAS) $$ 2-PENTEN-4-OL $$ Methyl prop... 71 43

5000 ■ ' 1 i 1 TTrunII । 6 i ITT"u r i । 5.40 5.80 6.00 5.60 m/ z 71.00 80.78% 53 58 67 86 " 111■ ‘ i " " r '" i' TTI । > 111111»111 THIHTTH 1 " I " " I'1" J " 11111' I m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4043: 3-Penten-2-ol (CAS) $$ 2-PENTEN-4-OL $$ Methyl prop... 43 71 ......... N. . 1 ' r । 1 ' 1 ■ । ■ ■ ' 1 r1 1 1 1 । 1 ' 1 ' । 5.40 5.60 5.80 6.00 5000 27 m/z 39.10 49.43%

15 53 31 58 67 | 35 - 86 i ■' ■ ■ i i1 ■ " i' 11 ++ —mTTTTTT m/z-> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 #3392:3-[.beta.-hydroxy-(.beta.,.beta.-dideuterio)lethylp... 71 85 90 -r-r-f-r-r-r-r-p-r 5.40 5.60 A 5.80 11 T'1 6.00 -

m/z 69.10 40.14%

5000 58 85 68 53 44 — 1111 11111111! 4 nImPTTTTTTT i11" i111' ' i'' " I ..... vr) A i' h ' ' — m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 5.40 5.60 5.80 6.00

)0613.D SCAN508.M Wed Jan 30 09:02:09 2002 Page 8

NYC-WTC_000051597

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NYC-WTC_000051597Source: NYC Law Department, mirrored locally

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