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GCMS analysis results for sample AE00613, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.

NYC-WTC_000051586–000051604

Folder label: “GCMS X 1/9/02 A 1/29/02

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Scanned page image, NYC-WTC_000051596
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN29\00613.D Vial: 2 . Acq On : 29 Jan 2002 3:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 2-Furanol, tetrahydro-2-met... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 5.02 0.14 ug/L 71248 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Furanol, tetrahydro-2-methyl- 102 C5H10O2 007326-46-7 45 2 2 - Furanmethanol , tetrahydro- 102 C5H10O2 000097-99-4 45 3 TETRAHYDRO-2 -METHYL-2 -FURANOL 102 C5H10O2 000000-00-0 45 4 Butenol, methyl- 86 C5H10O 060766-00-9 42 Abundance Scan 144 (5,018 min): 00613.D (-) m/z 71.10 100.00% 43 71

5000

■ । * ■ *' । vAL X- 39

■1 • ।11 ■ ■ ।111 I 55 59

' i11 — 86 ri'111111 UTTTTTT AA 4.60 m/ z 4.80 43.10 \ 5.00 5.20 5.40 94.16% /z—> 20 25 30 35 40 50 55 60 65 45 70 75 80 85 90 Abundance #9386:2-Furanol, tetrahydro-2-methyl- 71

5000 43 A nA,AA, MaAyA, 4.60 4.80 5.00 5.20 5.40 m/ z 41.10 52.52%

m/z-> -AL 49"50। "5555I" "6061r 11।" 20 25 30 35 . " 11 1,. । PPi 184.. mr 65 70 40 45 75 80 85 90 Abundance #9376: 2-Furanmethanol, tetrahydro- 711 43 4.60 . 4.80 A A A./ 5.00 5.20 5.40 5000 m/z 69.10 35.07% 27 31 53 57 61 T TTIIT I ''' 111 ■ ■ i ■1 ■ ■ i ■ ■ ■11 NTmTTT

miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #9405: TETRAHYDRO-2-METHYL-2-FURANOL -A- , , । ‘ r , rf-m 7h 4.60 4.80 5.00 5.20 5.40 m/z 55.10 27.53% 5000 43

- 49 55 61 "I" "I""!1 "'I' — 1..... 84 AA m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.60 4.80 5.00 5.20 5.40

30613.D SCAN508.M Wed Jan 30 09:02:09 2002 Page 7

NYC-WTC_000051596

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NYC-WTC_000051596Source: NYC Law Department, mirrored locally

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