GCMS analysis results for sample AE00027, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\O2 JAN25\00027.D Vial: 3 , Acq On : 25 Jan 2002 4:47 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* * Peak Number 5 Furan, tetrahydro-2-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

4.63 0.10 ug/L 42776 1,4-Dichlorobenzene-d4 9.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Furan, tetrahydro-2-methyl- 86 C5H10O 000096-47-9 38 2 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 35 3 Butanoic acid, 2-methyl-, methyl... 116 C6H12O2 000868-57-5 35 4 Butanoic acid, 2-methyl-, methyl... 116 C6H12O2 000868-57-5 35 Abundance Scan 110 (4.629 min): 00027.D (-) m/z 71.00 100.00% 41 71 57 88

5000 101 ‘1 1 * 4.20 4.40 4.60 4.80 5.00 51 m/z 41.00 91.94% ■ ■ i ■ ■ ■ ■ i 1 ‘ ■ 1 i ■ ■ TTHT i‘ 1 1 1 1 1 1 iz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #4155: Furan, tetrahydro-2-methyl- 43 71

5000 27 AH A 4.20 4.40 4.60 4.80 5.00 15 56 m/z 57.10 75.90% 86 Try. I. '. r mm miz-> 10 20 30 50 40 60 70 80 90 100 110 Abundance #4076:2-Buten-1-ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 71 i ■ ■ ■ ■ i ■ ■ ■ 1 i ' 1 b I 1. 1'"' 1 41 4.20 4.40 4.80 5.00 4.60 5000 m/z 88.00 71.47% 53 86 27

i 1 1 1 1 i 1 1 1 ■ i 1 1 1 .11 . • h . । । । । . । । ।—’. '. ■. r. I. ■..r ■ i ■ 1 1 ' i ' 1 1 1 i iz-> 10 20 30 40 50 70i 60 80 90 100 110 Abundance #16439: Butanoic acid, 2-methyl-, methyl ester (CAS) $$ Me... TTTunTT’Trt—u’ 57 88 4.20 4.40 4.60 4.80 5.00 m/z 43.10 57.94% 41 5000

101

m/z—> I ' ‘ 1 ' I 1 ' 1 ' I 1 1 1 1 I 1 ' ■ ’I 1 10 20 30 40 50 lp 60 69 .Pr 70 .,.— 80 90 i 1 ' ■ 1 i 1 1 ‘ ' I 100 110 /AAA.ANANAW 4.20 4.40 4.60 4.80 5.00

00027.D SCAN508.M Mon Jan 28 09:49:29 2002 Page 7

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