GCMS analysis results for sample AE03245, March 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03245.D Vial: 6 • Acq On : 1 Mar 2002 2:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 7 Butenol, methyl- Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 5.02 0.09 ug/L 41616 1,4-Dichlorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Butenol, methyl- 86 C5H10O 060766-00-9 59 2 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 59 3 2-Furanmethanol, tetrahydro- (CA... 102 C5H10O2 000097-99-4 47 4 3-Buten-2-ol, 2-methyl-____________ 86 C5H10O 000115-18-4 38 Abundance Scan 146 (5.022 min): 03245.D (-) m/z 71.00 100.00% 43 71

5000 59

51 55 1 444 84 4.60 4.80 5.00 5.20 5.40

m/z-> 5 ob .Jill... 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 " i"" i1" L’1111"" i m/ z 43.10 93.22% Abundance #4093: Butenol, methyl- 43 71

5000- 27 59 MwwN AA4 15 31 53

niz-> 5 0b ■111 ■ " i " 11 r ‘ 1 " r 1 “ i —HH ..67I 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 11/11111111186,,... Abundance #4081:3-Buten-2-ol, 2-methyl- (CAS) $$ 2-Methyl-3-buten-2... 71 M, , 7 43 4.60 4.80 5.00 5.20 5.40 5000 m/z 59.00 44.60% 59

■n/z-> Abundance 27 31

Ob ‘" 11 “' I'' ‘' I' “ ' I* 5 k r 1111111 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 53 67 L HH ........ 86..... #9384:2-Furanmethanol, tetrahydro- (CAS) $$ Tetrahydrofur...

43 7h A k I ’ 1 ■ 1 I 1 1 4.60 4.80 5.00 m/Z 69.10 5.20 5.40 40.92%

5000 27 31

m/z—> ob 1111111——111U70I7T 1II ■ "I 'I "I' 37 53 1................... Il ।11111 " I "" 11111111111 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 N... 1., 4.60 4.80 5.00 5.20 5.40

)3245.D HP022102.M Mon Mar 04 12:33:06 2002 Page 9

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