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GCMS analysis results for sample AE03245, March 2002

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03245 conducted on March 15, 2002.

NYC-WTC_000006085–000006104

Folder label: “GCMS X 2/12/02 A 3/01/02

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Scanned page image, NYC-WTC_000006098
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03245.D Vial: 6 • Acq On : 1 Mar 2002 2:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************* * *** * * * ***************** Peak Number 8 3-Hexanol (CAS) $$ Hexan-3-... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

5.53 0.07 ug/L 29253 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol (CAS) $$ Hexan-3-ol $$... 102 C6H140 000623-37-0 9 2 Silane, trimethyl- (CAS) $$ Trim... 74 C3H10Si 000993-07-7 9 3 2-Methyl-2, 3-pentanediol 118 C6H1402 007795-80-4 9 4 2-Methyl-2,3-pentanediol 118 C6H14O2 007795-80-4 9 Abundance Scan 191 (5.530 min): 03245.D (-) m/z 59.00 100.00% 53

5000 43 207 V -G- N ■ ■ i PA 1

n/z-> 0- l. 84 ' i"" irl"i"" r‘"i"" i" " i " " i" " i'1" r ■"i" "r■" r"■ i"' ‘ r" 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 5.20 5.40 5.60 5.80 m/ z ■43.10 36.77% Abundance #9598:3-Hexanol (CAS) $$ Hexan-3-ol $$ C2H5CH(OH)C3H7 $$ ... 50

73 5000 31 43 5.20 5.40 5.60 5.80 m/z 41.10 22.03% 84 0- " i ■"' i" ■ ■ i ■ ‘T i'1" 11'111" " I" " i" " i" " i" " r'" i" " i" " i" " i" " r ■'11" ■ miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #2043: Silane, trimethyl- (CAS) $$ Trimethylsilane $$ 2-Me... 50 3177117112111 17P’ p । । |” 5.20 5.40 5.60 5.80 73 m/z 207.00 18.96% 5000 43

15 31 0 i I hj z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #17882:2-Methyl-2,3-pentanediol ■ ' । 1 ‘ । 59 5.20 5.40 5.60 5.80 m/z 45.00 13.81%

5000 43

m/z-> 0 J. ....................... 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190200210 5.20 5.40 5.60 5.80

3245.D HP022102.M Mon Mar 04 12:33:06 2002 Page 10

NYC-WTC_000006098

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NYC-WTC_000006098Source: NYC Law Department, mirrored locally

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