GCMS analysis results for sample AE00613, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN29\00613.D Vial: 2 Acq On : 29 Jan 2002 3:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************* * * * *** * * **** Peak Number 8 2-Propanol, 1-(2-methoxypro. .. Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

9.85 0.16 ug/L 83995 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 64 2 3-Hexanol (CAS) $$ Hexan-3-ol 102 C6H140 000623-37-0 38 3 Allyldimethylsilane $$ Silane, d... 100 C5H12Si 003937-30-2 9 4 3-Hexanol (CAS) $$ Hexan-3-ol $$... 102 C6H14O 000623-37-0 9 Abundance Scan 567 (9.847 min): 00613.D (-) m/ z 59.10 100.00% 59

5000

73 . 104 9.60 9.80 10.00 10.20 5t. =L4=====---=-=---=== m/z 58.10 9.83% mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #43942:2-Propanol, 1-(2-methoxypropoxy)- $$ 1-(2-Methoxyp... 59

— 5000 9.60 9.80 10.00 10.20 m/z 104.10 9.62% 31 45 73 104 .... I ■ i ' '1 ' i ■ - .1........ 1,1...... 130. 1 i 1 ' ' ■ i 1 ' ' ' i ' 1 ■ ■ i ■ 1 ' 1 i ■ ■ ■ 1 i ■ ■ ' ■ i ‘ 1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #9592: 3-Hexanol (CAS) $$ Hexan-3-ol 59 11 I 1 1 1 1 1' 1 17 9.60 9.80 10.00 10.20 31 m/ z 73.10 9.46% 5000 73

45 ■i' 1 1 ■ 1' 1 1 ■ i 1 111 ■ i ' ■ +I'l " ITT 84.................... miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #8170: Allyldimethylsilane $$ Silane, dimethyl-2-propenyl- 59 44 -A- - 9.80 10.00 10.20 9.60 m/ z 43.10 8.95%

5000

72 85 45 | 100 > l ■ 1 > 1 C 1 ' • ■ I 1 I11 • I i ■ .Jh . . . . I , ----- m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 9.60 9.80 10.00 10.20

30613.D SCAN508.M Wed Jan 30 09:02:09 2002 Page 10

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