GCMS analysis results for sample AE00613, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.

NYC-WTC_000051586–000051604

Folder label: “GCMS X 1/9/02 A 1/29/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN29\00613.D Vial: 2 - Acq On : 29 Jan 2002 3:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Acetic acid, 3 - [1,3]dioxola ... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.89 3.50 ug/L 1795750 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ . .. 174 C8H14O4 015745-87-6 33 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 1-Propene-1-thiol 74 C3H6S 000925-89-3 9 Abundance Scan 220 (5.885 min): 00613.D (-) m/z 73.10 100.00% 73

5000 43 r i < । i i , |-ri i । । । । । r- 5.60 5.80 6.00 6.20 । । 55 '"i" ........ . .... ....... **pm)PuuuODTpT .। 87 103 m/ z 43.05 25.11% J'1'11 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3Jdioxolan-2-ylpropyl ester 73

J 5000 ■ r i. 1 1 1 ' n^'1 1 i' 1 5.60 5.80 6.00 6.20 43 m/z 45.10 10.09% 27 55 87 TTTTTTTTT r ’ " i " ■' i' Hpni1 " ■ r " ' 113 174 i' " ' 1111' i1 " ' r " ' i1' " r ' " i1 " 11 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 *1100,) 5.60 5.80 6.00 6.20 5000 m/ z 41.10 ~ 9.23% 43 27 55 . 87 113 174 " l" " I " i' TNITT -po TT 11"11 i ■ ■" i'1' ■ i ■ ‘' i i ‘' i' m/z~> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... - , , | M Ji m eri | i — 30 5.60 5.80 6.00 6.20 73 m/z 71.10 6.73%

5000 44 58

m/z—> 15 —10P Hpr TIF i''111'11' i " ■ ■ i' " • r1" i11" r 1' ■ i ■ " ' i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Ti l' " 11' ’ " I " ' TTT . Mp—.P 5.60 5.80 6.00 6.20

)0613.D SCAN508.M Wed Jan 30 09:02:09 2002 Page 9

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