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GCMS analysis results, sample AE00738, January 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AE00738 conducted on 1/29/02, detecting unknown compounds and 2,4-DDD surrogate at 99 ug with 5.0 MDL.

NYC-WTC_000051948–000051966

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00738.D vial: 6 . Acq On : 16 Jan 2002 7:17 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 2-Propanol, 1-(2-methoxypro... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

9.84 0.31 ug/L 107220 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 83 2 PROPYLENE GLYCOL TRIMER 1 174 C9H18O3 000000-00-0 43 3 PROPYLENE GLYCOL TRIMER 3 174 C9H18O3 000000-00-0 40 4 3-Hexanol (CAS) $$ Hexan-3-ol $$... 102 C6H14O 000623-37.-0 39 Abundance Scan 566 (9.836 min): 00738.D (-) m/z 59.10 100.00% 50

5000

0- 45 .............. ................. .... 73 I. 104 9.40 m/z til 9.60 45.10 9.80 ‘ ’ i' ' 10.00 10.20 11.85% n/z-> 30 40 50 7060 80 90 130 100 110 120 Abundance #43942: 2-Propanol, 1-(2-methoxypropoxy)- $$ 1-(2-Methoxyp... 50

5000 ■ ' i ■ ■

9.40 9.60 9.80 10.00 10.20 m/ Z 73.10 9.18% 31 45 0- ----- ,, J3 . . 194 , 130, m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #78532: PROPYLENE GLYCOLTRIMER 1 50 ....... 4... 9.40 9.60 9.80 10.00 10.20 5000 41 m/z 43.10 8.53% 103

| 73 87 ,.............. 117 130 0- ■ ■ i ■ IIPl, — ■ i ■ ■ i • < m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #78534: PROPYLENE GLYCOL TRIMER 3 50 9.40 9.60 9.80 10.00 10.20 m/z 42.10 8.33%

5000 41 I 103

m/z-> o 1 1 I 1 1 1 "T 11 1 1 1 30 40 50 73 At 60 70 80 87

90 100 110 117 120 130 130 9.40 A/N Ma... 9.60 9.80 10.00 10.20

)0738.D SCAN508.M Thu Jan 17 08:17:47 2002 Page 9

NYC-WTC_000051960

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NYC-WTC_000051960Source: NYC Law Department, mirrored locally

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