GCMS analysis results for sample AE00613, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.

NYC-WTC_000051586–000051604

Folder label: “GCMS X 1/9/02 A 1/29/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN29\00613.D Vial: 2 ■ Acq On : 29 Jan 2002 3:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ******************************************************************** * Peak Number 9 Cyclopentasiloxane, decamet... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

12.54 0.14 ug/L 97365 Naphthalene-d8 13.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 64 3 2,6-DIHYDROXYBENZOIC ACID 3TMS $... 370 C16H30O4Si3 003782-85-2 38 4 Benzoic acid, 2-[(trimethylsilyl... 282 C13H2203Si2 003789-85-3 38 Abundance Scan 803 (12.542 min): 00613.D (-) m/z 73.10 100.00% 73

5000 267 355 < । I • 1 ..... । । ■ ' i T 45 193 12.20 12.40 12.60 12.80 L 154 339 • । ■ ■ ■ ■ । ■ ■ ■ । ■ ■ i ■ ■ ■11 ■ ■ ■ ■ i ■ ■i " ' ■ i ■ ■ ■ ■ i ■ ■ ■' i • ■1 ■ i ■ ‘IT ■' ‘1 ’ m/z 267.00 43.01% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267. 5000 12.20 12.40 12.60 12.80 m/z 355.10 35.62%

m/z-> ■ i1 ■ ■ ■ । ■ i •1'11 • ■ ■' i • ■ ■ ■ j 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 191207 ■ * ► i ‘ * ir * •' i XU 323339 ' i'1''' r T‘3

Abundance #313065: Cyclopentasiloxane, decamethyl- 73 ■ ■ i ■ > ■ ■ । । T 1220 12.40 12.60 12.80 5000 267 m/z 356.10 14.30% 355 45 ........... 1 " 1'i ■ ................................ 193 223 251 - TIPBIIenn 323339 J ————n‘i '■ i i1 ■ ■' i1'1' i'' " r " ' i " '' i " 1' i ■ " ' i " i " 1' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313258: 2,6-DIHYDROXYBENZOIC ACID 3TMS $$ trimethylsilyl ... T 1 r1 1 1 73 12.20 12.40 12.60 12.80 355 m/z 268.00 10.15%

5000 45 147 267 27249 TT‘1‘19‘t-s‘"‘1‘‘1111111"11‘11**1‘11111111111110‘1117‘11TTT‘TTTT"""‘TTG‘T ‘LT • ■ । ■ • ■ ■ । ■ i ■ ■ ■ ■ i ' ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 1220 12.40 12.60 12.80

30613.D SCAN508.M Wed Jan 30 09:02:09 2002 Page 11

NYC-WTC_000051600

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NYC-WTC_000051600Source: NYC Law Department, mirrored locally

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