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GCMS results for sample AE00468, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00468 with surrogate recovery data on January 18, 2002.

NYC-WTC_000051318–000051335

Folder label: “GCMS X 1/8/02 A 1/10/02

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Scanned page image, NYC-WTC_000051325
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN10\00468.D Vial: 5 Acq On : 10 Jan 2002 6:07 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 9.54 0.18 ug/L 59307 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methy. . . 148 C7H16O3 020324-32-7 74 2 2-Propanol, 1,1'-oxybis- (CAS) $... 134 C6H14O3 000110-98-5 50 3 DIPROPYLENEGLYCOL METHYL ETHER $... 148 C7H16O3 020324-32-7 39 4 3-Hexanol (CAS) $$ Hexan-3-ol $$... 102 C6H14O 000623-37-0 33 Abundance Scan 540 (9.539 min): 00468.D (-) m/z 59.10 100.00% 59

5000 45 103 73

84 9.20 9.40 9.60 9.80 , 1 - 1— 01 . m/z 45.10 47.69% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #43943: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- $$ Dipro... 50

5000 -................................... 45 103 9.20 9.40 9.60 9.80 73 31 m/z 103.10 35.24% । 130 0- 1 ruu ------- — PPt ■ i ■ ' ■ ' i ■ ' ■ 1 i ' ' ■ ' i ' ' ■ ■ i ■ ■ ' ‘ i ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #29204:2-Propanol, 1,1 '-oxybis- (CAS) $$ Dipropylene glyc... 59

9.20 9.40 9.60 9.80 31 m/z 73.10 27.83% 5000 45 103

m/z-> Abundance O—TT 10 ' i ' 1 ■ ' i ' ' ■ ■ 1’’’ ■ i ■ —4 i ' ' ' 1 i ' 1 ■ ' i 1 ■ ■ ' i ' 1 ■ ■ I 1 1 1 ' i ' ■ ■ ■ i ■ ■ ■ ■ i ' 1 20 30 40 50 60 70 #43944: DIPROPYLENEGLYCOL METHYL ETHER $$ 2-Propanol, 1-(2... 59 80 90 100 110 120 130 . ... NN A 9.20 9 40 9.60 9.80 103 m/z 41.00 23.85%

5000 45 73 31 15 130 o ' ' I 1 ''' 11 1 1 ' 1 1 1-- ------PPP T ................. .. I ' ' TT m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 9 20 9.40 9.60 9.80

30468.D SCAN508.M Fri Jan 11 10:08:42 2002 Page 4

NYC-WTC_000051325

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NYC-WTC_000051325Source: NYC Law Department, mirrored locally

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