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GCMS analysis results for sample AE00108, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.

NYC-WTC_000050754–000050773

Folder label: “GCMS X 1/4/02 A 1/25/02

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NYC 9/11 Public Portal Document i WB/8 *** **L

Data File : C: \MSDCHEM\1\5973N\02JAN25\00108.D Vial: 6 Acq On : 25 Jan 2002 2:18 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2-Propanol, 1-(2-methoxy-1-... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

9.63 0.22 ug/L 101465 1,4-Dichlorobenzene-d4 9.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy-1-methy... 148 C7H16O3 020324-32-7 83 2 2-Propanol, l,l'-oxybis- (CAS) $... 134 C6H1403 000110-98-5 64 3 DIPROPYLENEGLYCOL METHYL ETHER $... 148 C7H1603 020324-32-7 56 4 BIS(1-METHYL-2-HYDROXYETHYL)ETHER 134 C6H14O3 000000-00-0 50 Abundance Scan 548 (9.630 min): 00108.D (-) m/z 59.10 100.00% 59

.. M. 5000 45 103 73 1 I ' ' 9.20 -p-PPPTP 39 > 84 ' I ■ ■ ■ ■ i ' ||1 ' ■ i' ■ i ■' ■' i' ‘ m/ z 45.10 45.88% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120' 130 Abundance #43943:2-Propanol, 1-(2-methoxy-1 -methylethoxy)- $$ Dipro...

5000

31 45 59

73 103 14 9.20 9.40 9.60 ' 9.80/10.00 m/z 103.0534.16% A

1 ■ i11111 ■111 ei 1111 >i 111 TH i'" i r '"i.'.’.PPITT i • * ’ k i • • ■ 130 ’ i 1 ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #29204: 2-Propanol, 1,1‘-oxybis- (CAS) $$ Dipropylene glyc... 59 ' i 1 1 ■ ' i 1 1 1 1 I 1 ' 9.20 9.40 9.60 9.80 10.00 31 m/z 73.10 27.42% 5000 45 103

' ' I 1 • > • | । ’ T""l

Abundance 10#43944.81PROPYLENEGLYcoLMETHYL 59 -P+ j > ■ • ■ । < < ■ < | ETER $S%2.prOpanol0(2.30 ‘ | 1 ‘ ' I ’ ■ ■ ’ I ■ ' ' ' I ’ ‘ ' t ‘ •

9.20 9.60 m/z 9.4041.10 MMA 9.80 10.00 23.17% 103

NW, 5000 45 73 31

m/z—> 1 1 ‘ 10 15 'I ' 1 1 ‘I ' 20 30 1 11 ' ' ' I ' • ' ' I' • ' ' I 1 ' '1 I 1 ' '' I 1 1 1 1 I 1 40 50 60 70 80 90 100 110 120 130 130 —4 9.20 9.40 9.60 9.80 10.00

00108.D SCAN508.M Mon Jan 28 09:50:00 2002 Page 11

NYC-WTC_000050768

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NYC-WTC_000050768Source: NYC Law Department, mirrored locally

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