Laboratory report showing GCMS analysis of sample AE00468 with surrogate recovery data on January 18, 2002.
NYC-WTC_000051318–000051335Folder label: “GCMS X 1/8/02 A 1/10/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C: \MSDCHEM\1\5973N\02JAN10\00468.D Vial: 5 Acq On 10 Jan 2002 6:07 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Muitiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 1 Acetic acid, 3-[1,3]dioxola... Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T. 5.89 4.02 ug/L 1338080 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 23-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 32 4 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 28 Abundance Scan 220 (5.886 min): 00468.D (-) m/ z 73.10 100.00% 73
m/z-> 5000
0-PTT 43
41R. । ----- 87 103 11,11' i 11 ■ ■ ■11 ■111111111 ‘ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ' i ■' ■' i1 r'11 ■ l r' ' I ' ' ' ' I ' ' ' ' 1’’ ' ' I ' ' ' ' m/z 5 60 5.80 6.00 6.20 43.10 24.67% Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73
5000 '1 ' rr i ■ 1 ' I ' ■ 1 ' i1′1117′4 5.60 5.80 6.00 6.20 43 m/z 45.10 9.47% 27 55 87 113 174 0-TTIPmTT 11" " i' " 1, 1 | Hypuidim I' " ' i " " I'1" i " " i " " i " " i " " i " " I " " i' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3‘-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 I I I I I I I ■> I I I / I 11B I I I I I I
5.60 5.80 6.00 6.20 5000 m/z 41.10 9.42% 43 27 55 87 113 174 0 TTIPTTTTTTTTT Tp ITT +TITOT TITmmnuOOT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4814: Silane, tetramethyl- 73 5.60 5.80 6.00 6.20 m/z 71.10 7.09%
5000
15 1 53 45 | 88 0 — i . r । I Pl i । i'i'.'I'i i . i 11 l1 l••j■• ■ >i ■ " ■ i■■'■i'■ ■ ’i■ ■ ■ ■ f ■ ■ • ■i■■■ ■ i' "• i’ ■ ■■i■ " 11' _ V >,।,। m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20
00468.D SCAN508.M Fri Jan 11 10:08:42 2002 Page 3
NYC-WTC_000051324
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NYC-WTC_000051740
GCMS analysis log for sample AE00560 showing surrogate recovery and unknown compounds detected on January 17, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050774
Laboratory report listing unknown compounds and surrogate recovery for sample AE00106 analyzed on February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050912
Laboratory record documenting GCMS surrogate recovery data for sample AE00281 analyzed on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052291
Laboratory report detailing GCMS scan results for sample AE00844, including detection of unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052251
Laboratory report showing GCMS analysis of sample AE00842 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052311
Laboratory report detailing GCMS scan results for sample AE00841, including detection of unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050893
Laboratory record documenting GCMS surrogate recovery data for sample AE00280 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050838
Quality control report for GCMS analysis of sample AE00277 showing surrogate recovery data from January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051549
Laboratory report showing GCMS analysis results for sample AE00556 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003543
Laboratory report documenting GCMS analysis of sample AE01141 conducted on February 27, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000051152
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051153
Document header page containing identification codes and metadata for GCMS files processed in early January 2002.
Filed in the same folder
NYC-WTC_000051156
Laboratory report detailing GCMS analysis of sample AE00327 for volatile organic compounds on January 10-11, 2002.
Filed in the same folder
NYC-WTC_000051165
Laboratory report showing GCMS analysis of reference standards used for calibration during January 10-11, 2002 testing.
Filed in the same folder
NYC-WTC_000051179
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 10-11, 2002 testing.
Filed in the same folder